S-(N-(9-fluorenylmethoxycarbonyl-N-phenylamino)methyl)-N-(2,4-dinitrophenyl)-cysteine

Base Information

Chemical Name:S-(N-(9-fluorenylmethoxycarbonyl-N-phenylamino)methyl)-N-(2,4-dinitrophenyl)-cysteine
CAS No.:1346434-16-9
Molecular Formula:C₃₁H₂₆N₄O₈S
Molecular Weight:614.635
Hs Code.:

Synonyms:S-(N-(9-fluorenylmethoxycarbonyl-N-phenylamino)methyl)-N-(2,4-dinitrophenyl)-cysteine

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Chemical Property of S-(N-(9-fluorenylmethoxycarbonyl-N-phenylamino)methyl)-N-(2,4-dinitrophenyl)-cysteine

Chemical Property:

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Technology Process of S-(N-(9-fluorenylmethoxycarbonyl-N-phenylamino)methyl)-N-(2,4-dinitrophenyl)-cysteine

There total 3 articles about S-(N-(9-fluorenylmethoxycarbonyl-N-phenylamino)methyl)-N-(2,4-dinitrophenyl)-cysteine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₄H₃₀N₄O₈S

: 1346434-16-9
S-(N-(9-fluorenylmethoxycarbonyl-N-phenylamino)methyl)-N-(2,4-dinitrophenyl)-cysteine

Guidance literature:: C₃₄H₃₀N₄O₈S; With phenylsilane; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 20 ℃; for 0.166667h;

With acetic acid; In ethyl acetate;

Reference yield:

: 1346434-13-6
O-(9-fluorenylmethyl)-N-phenyl-N-chloromethyl carbamate

: 1346434-16-9
S-(N-(9-fluorenylmethoxycarbonyl-N-phenylamino)methyl)-N-(2,4-dinitrophenyl)-cysteine

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 1 h

2: phenylsilane / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 0.17 h / 20 °C

With phenylsilane; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; dichloromethane;

Reference yield:

: 1346434-15-8
N-(DNP)-cysteine allyl ester

: 1346434-16-9
S-(N-(9-fluorenylmethoxycarbonyl-N-phenylamino)methyl)-N-(2,4-dinitrophenyl)-cysteine

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 1 h

2: phenylsilane / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 0.17 h / 20 °C

With phenylsilane; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; dichloromethane;