trifluoromethanesulfonic acid 4-[3-(tert-butyldiphenylsilanyloxy)propyl]-oxazol-2-yl ester

Base Information

Chemical Name:trifluoromethanesulfonic acid 4-[3-(tert-butyldiphenylsilanyloxy)propyl]-oxazol-2-yl ester
CAS No.:468774-15-4
Molecular Formula:C₂₃H₂₆F₃NO₅SSi
Molecular Weight:513.61
Hs Code.:

Synonyms:trifluoromethanesulfonic acid 4-[3-(tert-butyldiphenylsilanyloxy)propyl]-oxazol-2-yl ester

Suppliers and Price of trifluoromethanesulfonic acid 4-[3-(tert-butyldiphenylsilanyloxy)propyl]-oxazol-2-yl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of trifluoromethanesulfonic acid 4-[3-(tert-butyldiphenylsilanyloxy)propyl]-oxazol-2-yl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of trifluoromethanesulfonic acid 4-[3-(tert-butyldiphenylsilanyloxy)propyl]-oxazol-2-yl ester

There total 8 articles about trifluoromethanesulfonic acid 4-[3-(tert-butyldiphenylsilanyloxy)propyl]-oxazol-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 468774-17-6
4-[3-(tert-butyldiphenylsilanyloxy)propyl]-3H-oxazol-2-one

: 468774-15-4
trifluoromethanesulfonic acid 4-[3-(tert-butyldiphenylsilanyloxy)propyl]-oxazol-2-yl ester

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at -78 - 20 ℃; for 0.5h;
DOI:10.1021/jo0610412

Reference yield:

: 132047-92-8
tert-butyl(pent-4-en-1-yloxy)diphenylsilane

: 468774-15-4
trifluoromethanesulfonic acid 4-[3-(tert-butyldiphenylsilanyloxy)propyl]-oxazol-2-yl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 95 percent / OsO₄; TMANO / acetone; H₂O

2: 95 percent / H₂O₂; pyridinium peroxotungstophosphate / CH₂Cl₂ / Heating

3: N,N-dimethylaniline / toluene

4: NH₄OH / H₂O

5: H₂SO₄

6: 80 percent / 2,6-lutidine / CH₂Cl₂ / 0.5 h / -78 - 20 °C

With 2,6-dimethylpyridine; ammonium hydroxide; osmium(VIII) oxide; trimethylamine-N-oxide; pyridinium peroxotungstophosphate; sulfuric acid; dihydrogen peroxide; N,N-dimethyl-aniline; In dichloromethane; water; acetone; toluene;
DOI:10.1021/jo0610412

Reference yield:

: 468774-16-5
5-(tert-butyldiphenylsilanyloxy)-1-hydroxypentan-2-one

: 468774-15-4
trifluoromethanesulfonic acid 4-[3-(tert-butyldiphenylsilanyloxy)propyl]-oxazol-2-yl ester

Guidance literature:: Multi-step reaction with 4 steps

1: N,N-dimethylaniline / toluene

2: NH₄OH / H₂O

3: H₂SO₄

4: 80 percent / 2,6-lutidine / CH₂Cl₂ / 0.5 h / -78 - 20 °C

With 2,6-dimethylpyridine; ammonium hydroxide; sulfuric acid; N,N-dimethyl-aniline; In dichloromethane; water; toluene;
DOI:10.1021/jo0610412