C₂₂H₂₆N₂O₃

Base Information

• Chemical Name: C₂₂H₂₆N₂O₃
• CAS No.: 1278574-96-1
• Molecular Formula: C₂₂H₂₆N₂O₃
• Molecular Weight: 366.46
• Mol file: 1278574-96-1.mol

Synonyms:C₂₂H₂₆N₂O₃

Chemical Property of C₂₂H₂₆N₂O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₂H₂₆N₂O₃

There total 1 articles about C₂₂H₂₆N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

indole (120-72-9) + 1-nitro-1-heptene (150367-10-5,78346-64-2) + benzaldehyde (100-52-7) → C22H26N2O3 (1278574-96-1)

Guidance literature:

With copper (I) trifluoromethane sulfonate benzene; 1,1,1,3',3',3'-hexafluoro-propanol; 2-{[(1S)-N-{[(4S,5S)-4,5-dihydro-4,5-diphenyl-1-tosyl-1H-imidazol-2-yl]methyl}-1-phenylethanamino]methyl}-4,6-dibromophenol; In toluene; at 20 ℃; Inert atmosphere;

DOI:10.1021/jo1025833

Reference yield: 98.0%

C22H26N2O3 (1278574-96-1) → C22H28N2O (1278575-08-8)

Guidance literature:

With hydrogenchloride; acetic acid; zinc; In methanol; water; at 20 ℃; for 3h;

DOI:10.1021/jo1025833

Reference yield:

C22H26N2O3 (1278574-96-1) → C28H42N2OSi (1278575-16-8)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogenchloride; acetic acid; zinc / methanol; water / 3 h / 20 °C

2: 1H-imidazole / N,N-dimethyl-formamide / 1 h / 0 °C

With 1H-imidazole; hydrogenchloride; acetic acid; zinc; In methanol; water; N,N-dimethyl-formamide;

DOI:10.1021/jo1025833

upstream raw materials:

indole

1-nitro-1-heptene

benzaldehyde

Downstream raw materials:

C₂₈H₄₂N₂OSi

C₂₉H₃₂N₂O

C₂₂H₂₈N₂O