2-[2-(2-tert-Butoxycarbonylamino-3-phenyl-propionylamino)-benzoylamino]-benzoic acid

Base Information

Chemical Name:2-[2-(2-tert-Butoxycarbonylamino-3-phenyl-propionylamino)-benzoylamino]-benzoic acid
CAS No.:183206-34-0
Molecular Formula:C₂₈H₂₉N₃O₆
Molecular Weight:503.555
Hs Code.:

Synonyms:2-[2-(2-tert-Butoxycarbonylamino-3-phenyl-propionylamino)-benzoylamino]-benzoic acid

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Chemical Property of 2-[2-(2-tert-Butoxycarbonylamino-3-phenyl-propionylamino)-benzoylamino]-benzoic acid

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Technology Process of 2-[2-(2-tert-Butoxycarbonylamino-3-phenyl-propionylamino)-benzoylamino]-benzoic acid

There total 4 articles about 2-[2-(2-tert-Butoxycarbonylamino-3-phenyl-propionylamino)-benzoylamino]-benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 183206-27-1
2-[2-(2-tert-Butoxycarbonylamino-3-phenyl-propionylamino)-benzoylamino]-benzoic acid methyl ester

: 183206-34-0
2-[2-(2-tert-Butoxycarbonylamino-3-phenyl-propionylamino)-benzoylamino]-benzoic acid

Guidance literature:: With potassium hydroxide; In methanol; for 4h; Heating;

Reference yield:

: 49854-16-2
methyl 2-(2-aminobenzoylamino)benzoate

: 183206-34-0
2-[2-(2-tert-Butoxycarbonylamino-3-phenyl-propionylamino)-benzoylamino]-benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1) NEt₃, isobutyl chloroformate / 1) CH₂Cl₂, -10 deg C, 20 min, 2) CH₂Cl₂, r.t., 1 h, reflux, 3 h

2: 75 percent / KOH / methanol / 4 h / Heating

With potassium hydroxide; triethylamine; isobutyl chloroformate; In methanol;

Reference yield:

: 72367-10-3
2-(2-nitrobenzoylamino)benzoic acid methyl ester

: 183206-34-0
2-[2-(2-tert-Butoxycarbonylamino-3-phenyl-propionylamino)-benzoylamino]-benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / Zn, glac. HOAc / CH₂Cl₂ / 1 h / Ambient temperature

2: 1) NEt₃, isobutyl chloroformate / 1) CH₂Cl₂, -10 deg C, 20 min, 2) CH₂Cl₂, r.t., 1 h, reflux, 3 h

3: 75 percent / KOH / methanol / 4 h / Heating

With potassium hydroxide; acetic acid; triethylamine; zinc; isobutyl chloroformate; In methanol; dichloromethane;