4-amino>methyl>-N-<(phenylmethoxy)carbonyl>amino>butyl 6-<(tert-butyldimethylsilyl)oxy>-3-oxohexanoate

Base Information

Chemical Name:4-amino>methyl>-N-<(phenylmethoxy)carbonyl>amino>butyl 6-<(tert-butyldimethylsilyl)oxy>-3-oxohexanoate
CAS No.:150252-68-9
Molecular Formula:C₃₃H₄₇N₃O₈Si
Molecular Weight:641.837
Hs Code.:

4-<N-<imino<<(phenylmethoxy)carbonyl>amino>methyl>-N-<(phenylmethoxy)carbonyl>amino>butyl 6-<(tert-butyldimethylsilyl)oxy>-3-oxohexanoate

Synonyms:4-amino>methyl>-N-<(phenylmethoxy)carbonyl>amino>butyl 6-<(tert-butyldimethylsilyl)oxy>-3-oxohexanoate

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Chemical Property of 4-amino>methyl>-N-<(phenylmethoxy)carbonyl>amino>butyl 6-<(tert-butyldimethylsilyl)oxy>-3-oxohexanoate

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Technology Process of 4-amino>methyl>-N-<(phenylmethoxy)carbonyl>amino>butyl 6-<(tert-butyldimethylsilyl)oxy>-3-oxohexanoate

There total 3 articles about 4-amino>methyl>-N-<(phenylmethoxy)carbonyl>amino>butyl 6-<(tert-butyldimethylsilyl)oxy>-3-oxohexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 116585-05-8
methyl 6-<(tert-butyldimethylsilyl)oxy>-3-oxohexanoate

: 150252-67-8
4-[N-(imino{[(phenylmethoxy)carbonyl]amino}methyl)-N-[(phenylmethoxy)carbonyl]amino]butan-1-ol

: 150252-68-9
4-amino>methyl>-N-<(phenylmethoxy)carbonyl>amino>butyl 6-<(tert-butyldimethylsilyl)oxy>-3-oxohexanoate

Guidance literature:: dmap; In benzene; for 24h; Heating;
DOI:10.1021/jo00067a014

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 150252-68-9
4-amino>methyl>-N-<(phenylmethoxy)carbonyl>amino>butyl 6-<(tert-butyldimethylsilyl)oxy>-3-oxohexanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Me₃SiCl, DIPEA, 2.) DIPEA / 1.) 1,2-dichloroethane, 40 deg C, 1 h, 2.) a) 0 deg C, 20 min, b) room temperature, 40 h

2: 53 percent / DMAP / benzene / 24 h / Heating

With chloro-trimethyl-silane; N-ethyl-N,N-diisopropylamine; dmap; In benzene;
DOI:10.1021/jo00067a014

Reference yield:

: (4-hydroxybutyl)guanidinium toluenesulfonate

: 150252-68-9
4-amino>methyl>-N-<(phenylmethoxy)carbonyl>amino>butyl 6-<(tert-butyldimethylsilyl)oxy>-3-oxohexanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Me₃SiCl, DIPEA, 2.) DIPEA / 1.) 1,2-dichloroethane, 40 deg C, 1 h, 2.) a) 0 deg C, 20 min, b) room temperature, 40 h

2: 53 percent / DMAP / benzene / 24 h / Heating

With chloro-trimethyl-silane; N-ethyl-N,N-diisopropylamine; dmap; In benzene;
DOI:10.1021/jo00067a014