4-[N-(imino{[(phenylmethoxy)carbonyl]amino}methyl)-N-[(phenylmethoxy)carbonyl]amino]butan-1-ol

Base Information

Chemical Name:4-[N-(imino{[(phenylmethoxy)carbonyl]amino}methyl)-N-[(phenylmethoxy)carbonyl]amino]butan-1-ol
CAS No.:150252-67-8
Molecular Formula:C₂₁H₂₅N₃O₅
Molecular Weight:399.447
Hs Code.:

Synonyms:4-[N-(imino{[(phenylmethoxy)carbonyl]amino}methyl)-N-[(phenylmethoxy)carbonyl]amino]butan-1-ol

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Chemical Property of 4-[N-(imino{[(phenylmethoxy)carbonyl]amino}methyl)-N-[(phenylmethoxy)carbonyl]amino]butan-1-ol

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Technology Process of 4-[N-(imino{[(phenylmethoxy)carbonyl]amino}methyl)-N-[(phenylmethoxy)carbonyl]amino]butan-1-ol

There total 1 articles about 4-[N-(imino{[(phenylmethoxy)carbonyl]amino}methyl)-N-[(phenylmethoxy)carbonyl]amino]butan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: (4-hydroxybutyl)guanidinium toluenesulfonate

: 150252-67-8
4-[N-(imino{[(phenylmethoxy)carbonyl]amino}methyl)-N-[(phenylmethoxy)carbonyl]amino]butan-1-ol

Guidance literature:: With chloro-trimethyl-silane; N-ethyl-N,N-diisopropylamine; Yield given. Multistep reaction; 1.) 1,2-dichloroethane, 40 deg C, 1 h, 2.) a) 0 deg C, 20 min, b) room temperature, 40 h;
DOI:10.1021/jo00067a014

Reference yield: 92.0%

: 124-63-0
methanesulfonyl chloride

: 150252-67-8
4-[N-(imino{[(phenylmethoxy)carbonyl]amino}methyl)-N-[(phenylmethoxy)carbonyl]amino]butan-1-ol

: N¹,N²-bis(benzyloxycarbonyl)-N¹-(4-[(methanesulfonyl)oxy]butyl)guanidine

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 0.166667h;
DOI:10.1021/ol034042e

Reference yield: 75.0%

: 150252-67-8
4-[N-(imino{[(phenylmethoxy)carbonyl]amino}methyl)-N-[(phenylmethoxy)carbonyl]amino]butan-1-ol

: 345959-31-1
1-methoxy-3-(9-triisopropylsilanyloxy-nonyl)-3,5,6,7-tetrahydro-pyrrolo[1,2-c]pyrimidine-4-carboxylic acid

: 345959-32-2
C₄₈H₇₃N₅O₈Si

Guidance literature:: With bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine; In dichloromethane; at 20 ℃; for 18h;
DOI:10.1021/ol015848m