methyl (7S)-7-phenyl-4-fluoro-3,5-dimethoxy-2,6-dioxa-3,5-diphosphaoctan-8-oate-3,5-dioxide

Base Information

Chemical Name:methyl (7S)-7-phenyl-4-fluoro-3,5-dimethoxy-2,6-dioxa-3,5-diphosphaoctan-8-oate-3,5-dioxide
CAS No.:1375082-72-6
Molecular Formula:C₁₃H₁₉FO₈P₂
Molecular Weight:384.235
Hs Code.:

Synonyms:methyl (7S)-7-phenyl-4-fluoro-3,5-dimethoxy-2,6-dioxa-3,5-diphosphaoctan-8-oate-3,5-dioxide

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Chemical Property of methyl (7S)-7-phenyl-4-fluoro-3,5-dimethoxy-2,6-dioxa-3,5-diphosphaoctan-8-oate-3,5-dioxide

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Technology Process of methyl (7S)-7-phenyl-4-fluoro-3,5-dimethoxy-2,6-dioxa-3,5-diphosphaoctan-8-oate-3,5-dioxide

There total 2 articles about methyl (7S)-7-phenyl-4-fluoro-3,5-dimethoxy-2,6-dioxa-3,5-diphosphaoctan-8-oate-3,5-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1375082-70-4
sodium methyl[(dimethoxyphosphoryl)(fluoro)methyl]phosphonate

: 20698-91-3
(R)-methyl mandelate

: 1375082-72-6
methyl (7S)-7-phenyl-4-fluoro-3,5-dimethoxy-2,6-dioxa-3,5-diphosphaoctan-8-oate-3,5-dioxide

Guidance literature:: sodium methyl[(dimethoxyphosphoryl)(fluoro)methyl]phosphonate; In methanol;

(R)-methyl mandelate; With di-isopropyl azodicarboxylate; triphenylphosphine; In 1,4-dioxane; at 20 ℃; Inert atmosphere;
DOI:10.1021/ja300218x

Reference yield: 65.0%

: triethylammonium methyl [(dimethoxyphosphoryl)(fluoro)methyl]phosphonate

: 20698-91-3
(R)-methyl mandelate

: 1375082-72-6
methyl (7S)-7-phenyl-4-fluoro-3,5-dimethoxy-2,6-dioxa-3,5-diphosphaoctan-8-oate-3,5-dioxide

Guidance literature:: triethylammonium methyl [(dimethoxyphosphoryl)(fluoro)methyl]phosphonate;

(R)-methyl mandelate; With di-isopropyl azodicarboxylate; triphenylphosphine; In 1,4-dioxane; Inert atmosphere;
DOI:10.1021/ol503765n

Reference yield: 79.0%

: 1375082-72-6
methyl (7S)-7-phenyl-4-fluoro-3,5-dimethoxy-2,6-dioxa-3,5-diphosphaoctan-8-oate-3,5-dioxide

: methyl (2S)-({[fluoro(phosphono)methyl](hydroxy)phosphoryl}oxy)(phenyl)ethanoate

Guidance literature:: methyl (7S)-7-phenyl-4-fluoro-3,5-dimethoxy-2,6-dioxa-3,5-diphosphaoctan-8-oate-3,5-dioxide; With trimethylsilyl bromide; In acetonitrile;

With methanol;
DOI:10.1021/ol503765n