diethyl (acetylamino)<<3-(diethoxyphosphinyl)phenyl>methyl>propanedioate

Base Information

Chemical Name:diethyl (acetylamino)<<3-(diethoxyphosphinyl)phenyl>methyl>propanedioate
CAS No.:120667-46-1
Molecular Formula:C₂₀H₃₀NO₈P
Molecular Weight:443.434
Hs Code.:

Synonyms:diethyl (acetylamino)<<3-(diethoxyphosphinyl)phenyl>methyl>propanedioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl (acetylamino)<<3-(diethoxyphosphinyl)phenyl>methyl>propanedioate

Chemical Property:

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Technology Process of diethyl (acetylamino)<<3-(diethoxyphosphinyl)phenyl>methyl>propanedioate

There total 3 articles about diethyl (acetylamino)<<3-(diethoxyphosphinyl)phenyl>methyl>propanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 15017-44-4
diethyl (acetylamino)<(3-bromophenyl)methyl>propanedioate

: 762-04-9
phosphonic acid diethyl ester

: 120667-46-1
diethyl (acetylamino)<<3-(diethoxyphosphinyl)phenyl>methyl>propanedioate

Guidance literature:: With triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 90 ℃; for 5h;
DOI:10.1021/jm00127a030

Reference yield:

: 823-78-9
meta-bromobenzyl bromide

: 120667-46-1
diethyl (acetylamino)<<3-(diethoxyphosphinyl)phenyl>methyl>propanedioate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaOEt / 1.) EtOH, 15 min, 2.) THF, RT, overnight

2: 83 percent / triethylamine / tetrakis(triphenylphosphine)palladium⁽⁰⁾ / toluene / 5 h / 90 °C

With sodium ethanolate; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene;
DOI:10.1021/jm00127a030

Reference yield:

: 1068-90-2
2-acetylaminomalonic acid diethyl ester

: 120667-46-1
diethyl (acetylamino)<<3-(diethoxyphosphinyl)phenyl>methyl>propanedioate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaOEt / 1.) EtOH, 15 min, 2.) THF, RT, overnight

2: 83 percent / triethylamine / tetrakis(triphenylphosphine)palladium⁽⁰⁾ / toluene / 5 h / 90 °C

With sodium ethanolate; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene;
DOI:10.1021/jm00127a030