C₅₅H₇₇NO₁₀

Base Information

Chemical Name:C₅₅H₇₇NO₁₀
CAS No.:1574334-73-8
Molecular Formula:C₅₅H₇₇NO₁₀
Molecular Weight:912.217
Hs Code.:

C<sub>55</sub>H<sub>77</sub>NO<sub>10</sub>

Synonyms:C₅₅H₇₇NO₁₀

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Chemical Property of C₅₅H₇₇NO₁₀

Chemical Property:

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Technology Process of C₅₅H₇₇NO₁₀

There total 21 articles about C₅₅H₇₇NO₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.4%

: 1574334-69-2
C₄₂H₆₄O₇

: 1148-11-4
N-Benzyloxycarbonyl-L-proline

: 1574334-73-8
C₅₅H₇₇NO₁₀

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 - 20 ℃; for 2h;
DOI:10.1039/c3ob42364f

Reference yield:

: 92936-93-1
(4R,5S)-4-(bis(ethylthio)methyl)-5-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)-2,2-dimethyl-1,3-dioxolane

: 1574334-73-8
C₅₅H₇₇NO₁₀

Guidance literature:: Multi-step reaction with 8 steps

1.1: mercury(II) oxide; mercury dichloride / water; acetone / 60 °C

2.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 - 20 °C

3.1: acetic acid / water / 20 °C

4.1: triethylamine; di(n-butyl)tin oxide / dichloromethane / 20 °C

5.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 10 h / Reflux

6.1: n-butyllithium / tetrahydrofuran / 3 h / -78 - -20 °C

6.2: -78 °C

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 10 h / 20 °C

8.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 2 h / 0 - 20 °C

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; dmap; n-butyllithium; potassium tert-butylate; tetrabutyl ammonium fluoride; di(n-butyl)tin oxide; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; mercury dichloride; mercury(II) oxide; In tetrahydrofuran; dichloromethane; water; acetone;
DOI:10.1039/c3ob42364f

Reference yield:

: 90611-22-6
non-8-yn-al

: 1574334-73-8
C₅₅H₇₇NO₁₀

Guidance literature:: Multi-step reaction with 5 steps

1.1: (-)-Ipc₂BCl / diethyl ether / -100 °C / Inert atmosphere

2.1: 1H-imidazole / dichloromethane

3.1: n-butyllithium / tetrahydrofuran / 3 h / -78 - -20 °C

3.2: -78 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 10 h / 20 °C

5.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 2 h / 0 - 20 °C

With 1H-imidazole; dmap; n-butyllithium; (-)-Ipc₂BCl; tetrabutyl ammonium fluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1039/c3ob42364f