Bis(2,5-endomethylenecyclohexylmethyl)amine

Base Information

• Chemical Name: Bis(2,5-endomethylenecyclohexylmethyl)amine
• CAS No.: 10171-76-3
• Molecular Formula: C₁₆H₂₇N
• Molecular Weight: 233.397
• DSSTox Substance ID: DTXSID20906515
• Mol file: 10171-76-3.mol

Synonyms:10171-76-3;Bis(2,5-endomethylenecyclohexylmethyl)amine;DIMETHYLAMINE, 1,1'-DI-2-NORBORNYL-, endo,endo-;1-(2-bicyclo[2.2.1]heptanyl)-N-(2-bicyclo[2.2.1]heptanylmethyl)methanamine;(1R,4S)-N-[[(1S,4R)-Bicyclo[2.2.1]heptan-2alpha-yl]methyl]bicyclo[2.2.1]heptane-2beta-methanamine;bis(2-norbornylmethyl)amine;DTXSID20906515;Bicyclo[2.2.1]heptane-2-methanamine, N-(bicyclo[2.2.1]hept-2-ylmethyl)-, (endo,endo)-;AKOS018108240;LS-62029;1-(Bicyclo[2.2.1]heptan-2-yl)-N-[(bicyclo[2.2.1]heptan-2-yl)methyl]methanamine

Chemical Property of Bis(2,5-endomethylenecyclohexylmethyl)amine

Chemical Property:

• Vapor Pressure: 0.000728mmHg at 25°C
• Refractive Index: 1.5515 (estimate)
• Boiling Point: 307.4°C at 760 mmHg
• Flash Point: 134.9°C
• PSA: 12.03000
• Density: 1.002g/cm³
• LogP: 3.83930
• XLogP3: 4.4
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 4
• Exact Mass: 233.214349865
• Heavy Atom Count: 17
• Complexity: 259

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CC2CC1CC2CNCC3CC4CCC3C4

Technology Process of Bis(2,5-endomethylenecyclohexylmethyl)amine

There total 2 articles about Bis(2,5-endomethylenecyclohexylmethyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.5%

bicyclo[2.2.1]hept-5-ene-2-carbonitrile (95-11-4) → 2-Aminomethylbicyclo<2.2.1>heptane (14370-50-4) + di(2R-exo-norbornylmethyl)amine (10171-76-3,75442-89-6,75442-90-9,79731-57-0) + tris(2-norbornylmethyl)amine

Guidance literature:

With sodium tetrahydroborate; hydrogen; nickel dichloride; In isopropyl alcohol; at 70 ℃; for 12h; under 760.051 Torr;

DOI:10.1134/S1070363216020110

Reference yield:

→ di(2R-exo-norbornylmethyl)amine (10171-76-3,75442-89-6,75442-90-9,79731-57-0)

Guidance literature:

2-endo?-Aminomethyl-bicyclo<2,2,1>heptan;

upstream raw materials:

bicyclo[2.2.1]hept-5-ene-2-carbonitrile

Refernces