2,2'-(1,12-dodecylenedioxy)bis(5-nitrobenzaldehyde ethylene acetal)

Base Information

Chemical Name:2,2'-(1,12-dodecylenedioxy)bis(5-nitrobenzaldehyde ethylene acetal)
CAS No.:82542-47-0
Molecular Formula:C₃₀H₄₀N₂O₁₀
Molecular Weight:588.655
Hs Code.:

Synonyms:2,2'-(1,12-dodecylenedioxy)bis(5-nitrobenzaldehyde ethylene acetal)

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Chemical Property of 2,2'-(1,12-dodecylenedioxy)bis(5-nitrobenzaldehyde ethylene acetal)

Chemical Property:

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Technology Process of 2,2'-(1,12-dodecylenedioxy)bis(5-nitrobenzaldehyde ethylene acetal)

There total 3 articles about 2,2'-(1,12-dodecylenedioxy)bis(5-nitrobenzaldehyde ethylene acetal) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 107-21-1
ethylene glycol

: 82542-44-7
2,2'-(1,12-dodecylenedioxy)bis(5-nitrobenzaldehyde)

: 82542-47-0
2,2'-(1,12-dodecylenedioxy)bis(5-nitrobenzaldehyde ethylene acetal)

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 20h; Heating;
DOI:10.1016/0040-4020(82)85041-2

Reference yield:

: 3344-70-5
1,12-dibromododecane

: 82542-47-0
2,2'-(1,12-dodecylenedioxy)bis(5-nitrobenzaldehyde ethylene acetal)

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) aqueous sodium hydroxide / 2.) 120-130 deg C, DMF

2: 96 percent / p-toluene sulfonic acid / benzene / 20 h / Heating

With sodium hydroxide; toluene-4-sulfonic acid; In benzene;
DOI:10.1016/0040-4020(82)85041-2

Reference yield:

: 97-51-8
5-Nitrosalicylaldehyde

: 82542-47-0
2,2'-(1,12-dodecylenedioxy)bis(5-nitrobenzaldehyde ethylene acetal)

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) aqueous sodium hydroxide / 2.) 120-130 deg C, DMF

2: 96 percent / p-toluene sulfonic acid / benzene / 20 h / Heating

With sodium hydroxide; toluene-4-sulfonic acid; In benzene;
DOI:10.1016/0040-4020(82)85041-2