1,3-benzoxazol-2-yl 2-chlorobenzyl sulfide

Base Information

Chemical Name:1,3-benzoxazol-2-yl 2-chlorobenzyl sulfide
CAS No.:294873-29-3
Molecular Formula:C₁₄H₁₀ClNOS
Molecular Weight:275.759
Hs Code.:

Synonyms:2-((2-chlorobenzyl)thio)benzo[d]oxazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-benzoxazol-2-yl 2-chlorobenzyl sulfide

Chemical Property:

Boiling Point:419.3±47.0 °C(Predicted)
PKA:0.89±0.10(Predicted)
Density:1.37±0.1 g/cm3(Predicted)

Purity/Quality:

Safty Information:

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Technology Process of 1,3-benzoxazol-2-yl 2-chlorobenzyl sulfide

There total 4 articles about 1,3-benzoxazol-2-yl 2-chlorobenzyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 611-19-8
1-chloro-2-(chloromethyl)benzene

: 95-55-6
2-amino-phenol

: 294873-29-3
2-((2-chlorobenzyl)thio)benzo[d]oxazole

Guidance literature:: 2-amino-phenol; With Thiram; In water; at 120 ℃; Green chemistry;

1-chloro-2-(chloromethyl)benzene; With potassium carbonate; In water; at 80 ℃; for 1h; Green chemistry;
DOI:10.1021/acs.joc.8b02136

Reference yield: 78.0%

: 97-74-5
bis(dimethylthiocarbamoyl)sulfide

: 611-19-8
1-chloro-2-(chloromethyl)benzene

: 95-55-6
2-amino-phenol

: 294873-29-3
2-((2-chlorobenzyl)thio)benzo[d]oxazole

Guidance literature:: bis(dimethylthiocarbamoyl)sulfide; 2-amino-phenol; With sodium carbonate; In N,N-dimethyl-formamide; at 120 ℃; for 2h;

1-chloro-2-(chloromethyl)benzene; In N,N-dimethyl-formamide; at 60 ℃; for 1h;
DOI:10.1002/ejoc.202001214

Reference yield: 77.0%

: 2382-96-9,118090-08-7
2-sulfanyl-1,3-benzoxazole

: 294873-29-3
2-((2-chlorobenzyl)thio)benzo[d]oxazole

Guidance literature:: 2-sulfanyl-1,3-benzoxazole; With ethanol; sodium; In N,N-dimethyl-formamide; at 20 ℃; for 0.166667h; Inert atmosphere;

2-chlorobenzyl halide; In ethanol; N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.ejmech.2008.06.027