2-imino-4,5,5-trimethyl-3-phenyl-2,5-dihydrofuran hydrogen sulfate

Base Information

• Chemical Name: 2-imino-4,5,5-trimethyl-3-phenyl-2,5-dihydrofuran hydrogen sulfate
• CAS No.: 1290107-16-2
• Molecular Formula: C₁₃H₁₅NO*H₂O₄S
• Molecular Weight: 299.348
• Mol file: 1290107-16-2.mol

Synonyms:2-imino-4,5,5-trimethyl-3-phenyl-2,5-dihydrofuran hydrogen sulfate

Chemical Property of 2-imino-4,5,5-trimethyl-3-phenyl-2,5-dihydrofuran hydrogen sulfate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-imino-4,5,5-trimethyl-3-phenyl-2,5-dihydrofuran hydrogen sulfate

There total 1 articles about 2-imino-4,5,5-trimethyl-3-phenyl-2,5-dihydrofuran hydrogen sulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

2-imino-4,5,5-trimethyl-3-phenyl-2,5-dihydrofuran → 2-imino-4,5,5-trimethyl-3-phenyl-2,5-dihydrofuran hydrogen sulfate (1290107-16-2)

Guidance literature:

With sulfuric acid; In ethanol;

DOI:10.1134/S107042801102028X

Reference yield: 88.0%

2-imino-4,5,5-trimethyl-3-phenyl-2,5-dihydrofuran hydrogen sulfate (1290107-16-2) → 2-imino-4,5,5-trimethyl-3-phenyl-2,5-dihydrofuran

Guidance literature:

With potassium carbonate; In water; pH=7 - 8;

DOI:10.1134/S107042801102028X

Reference yield:

2-imino-4,5,5-trimethyl-3-phenyl-2,5-dihydrofuran hydrogen sulfate (1290107-16-2) → 3-phenyl-4,5,5-trimethyl-3(5H)-furanone (30982-21-9)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium carbonate / water / pH 7 - 8

2: hydrogenchloride / benzene

3: water / 3 h / Heating

With hydrogenchloride; water; potassium carbonate; In water; benzene;

DOI:10.1134/S107042801102028X

Downstream raw materials:

2-dicyanomethylene-4,5,5-trimethyl-3-phenyl-2,5-dihydrofuran

2-imino-4,5,5-trimethyl-3-phenyl-2,5-dihydrofuran hydrochloride

3-phenyl-4,5,5-trimethyl-3(5H)-furanone