Technology Process of diethyl 3,7-dioxa-5-(3-methoxybenzyl)-1,9-nonanedicarboxylate
There total 4 articles about diethyl 3,7-dioxa-5-(3-methoxybenzyl)-1,9-nonanedicarboxylate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 79 percent / LiAlH4 / diethyl ether / 2 h / Ambient temperature
2: 1.) potassium tert-butoxide / 1.) tert-butyl alcohol, RT, 1 h, 2.) tert-butyl alcohol, reflux, 15 h
3: p-toluenesulfonic acid / benzene / 6 h / Heating
With
lithium aluminium tetrahydride; potassium tert-butylate; toluene-4-sulfonic acid;
In
diethyl ether; benzene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) potassium tert-butoxide / 1.) tert-butyl alcohol, RT, 1 h, 2.) tert-butyl alcohol, reflux, 15 h
2: p-toluenesulfonic acid / benzene / 6 h / Heating
With
potassium tert-butylate; toluene-4-sulfonic acid;
In
benzene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) C2H5ONa / 1.) ethanol, 2.) ethanol a) RT, overnight, b) reflux, 8 h
2: 79 percent / LiAlH4 / diethyl ether / 2 h / Ambient temperature
3: 1.) potassium tert-butoxide / 1.) tert-butyl alcohol, RT, 1 h, 2.) tert-butyl alcohol, reflux, 15 h
4: p-toluenesulfonic acid / benzene / 6 h / Heating
With
lithium aluminium tetrahydride; potassium tert-butylate; sodium ethanolate; toluene-4-sulfonic acid;
In
diethyl ether; benzene;
![[(3-methoxyphenyl)methyl]propanedioic acid diethyl ester](/Databaselist/images/loading.webp)
