1,2-Bis(2,3-dimethoxyphenyl)ethanamine

Base Information

Chemical Name:1,2-Bis(2,3-dimethoxyphenyl)ethanamine
CAS No.:7148-04-1
Molecular Formula:C₁₈H₂₃NO₄
Molecular Weight:317.385
Hs Code.:
NSC Number:26678
DSSTox Substance ID:DTXSID60282587

Synonyms:7148-04-1;1,2-bis(2,3-dimethoxyphenyl)ethanamine;NSC26678;DTXSID60282587;NSC-26678

Suppliers and Price of 1,2-Bis(2,3-dimethoxyphenyl)ethanamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 1,2-Bis(2,3-dimethoxyphenyl)ethanamine

Chemical Property:

Vapor Pressure:1.88E-07mmHg at 25°C
Boiling Point:425.7°C at 760 mmHg
Flash Point:212.1°C
Density:1.119g/cm³
XLogP3:2.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:7
Exact Mass:317.16270821
Heavy Atom Count:23
Complexity:341

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=CC(=C1OC)CC(C2=C(C(=CC=C2)OC)OC)N

Technology Process of 1,2-Bis(2,3-dimethoxyphenyl)ethanamine

There total 4 articles about 1,2-Bis(2,3-dimethoxyphenyl)ethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 500285-76-7
2,3,2',3'-tetramethoxy-deoxybenzoin

: 7148-04-1
2,3,2',3'-tetramethoxy-bibenzyl-α-ylamine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium acetate; ethanol; hydroxylamine hydrochloride

2: sodium-amalgam; ethanol; acetic acid

With sodium amalgam; ethanol; hydroxylamine hydrochloride; sodium acetate; acetic acid;
DOI:10.1021/ja01225a060

Reference yield:

: 5653-61-2
2,3,2',3'-Tetramethoxy-benzoin

: 7148-04-1
2,3,2',3'-tetramethoxy-bibenzyl-α-ylamine

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol; coppered tin; concentrated aqueous hydrochloric acid

2: sodium acetate; ethanol; hydroxylamine hydrochloride

3: sodium-amalgam; ethanol; acetic acid

With hydrogenchloride; sodium amalgam; ethanol; coppered tin; hydroxylamine hydrochloride; sodium acetate; acetic acid;
DOI:10.1021/ja01225a060

Reference yield:

: 86-51-1
2,3-dimethyoxybenzaldehyde

: 7148-04-1
2,3,2',3'-tetramethoxy-bibenzyl-α-ylamine

Guidance literature:: Multi-step reaction with 4 steps

1: potassium cyanide; aqueous ethanol

2: ethanol; coppered tin; concentrated aqueous hydrochloric acid

3: sodium acetate; ethanol; hydroxylamine hydrochloride

4: sodium-amalgam; ethanol; acetic acid

With hydrogenchloride; potassium cyanide; sodium amalgam; ethanol; coppered tin; hydroxylamine hydrochloride; sodium acetate; acetic acid;
DOI:10.1021/ja01225a060