Dichlorodinitrosylmolybdenum

Base Information

• Chemical Name: Dichlorodinitrosylmolybdenum
• CAS No.: 44513-97-5
• Molecular Formula: 2Cl*Mo*2NO
• Molecular Weight: 226.858
• European Community (EC) Number: 256-158-8
• Mol file: 44513-97-5.mol

Synonyms:Dichlorodinitrosylmolybdenum;44513-97-5;EINECS 256-158-8;Cl2MoN2O2;Cl2-Mo-N2-O2

Chemical Property of Dichlorodinitrosylmolybdenum

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 34.14000
• Density: g/cm³
• LogP: -5.34760
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 0
• Exact Mass: 227.839086
• Heavy Atom Count: 7
• Complexity: 21.2

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: [N-]=O.[N-]=O.Cl[Mo]Cl

Technology Process of Dichlorodinitrosylmolybdenum

There total 1 articles about Dichlorodinitrosylmolybdenum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dichloro-bis(ethanol)-dinitrosylmolybdenum → Mo(2+)*2Cl(1-)*2NO=MoCl2(NO)2 (44513-97-5)

Guidance literature:

at 150°C;

Reference yield: 38.0%

Mo(2+)*2Cl(1-)*2NO=MoCl2(NO)2 (44513-97-5) + N-trimethylsilyl(triphenylphosphoranylidene)amine (13892-06-3) → [MoCl2(NO)2(triphenylphosphine oxide)2]

Guidance literature:

In acetonitrile; dry atm.; stirring, refluxing (2 h); evapn., washing (Et2O), crystn. (CH2Cl2, cooling, 2 d); elem. anal.;

Reference yield: 36.0%

Mo(2+)*2Cl(1-)*2NO=MoCl2(NO)2 (44513-97-5) + Triphenylphosphine oxide (791-28-6) → [MoCl3(NO)(OP(C6H5)3)2]*[MoCl4(OP(C6H5)3)2]=[MoCl3(NO)(OP(C6H5)3)2MoCl4(OP(C6H5)3)2]

Guidance literature:

In dichloromethane; dry atm.; molar ratio Mo compound:OPPh3 1:2, 0-20°C; crystn. (4°C, 3 d); elem. anal.;

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