[Mo3(η5-cyclopentadienyl)2(μ3-methylidyne)(μ-dicyclohexylphosphide)(CO)7]

Base Information

Chemical Name:[Mo3(η5-cyclopentadienyl)2(μ3-methylidyne)(μ-dicyclohexylphosphide)(CO)7]
CAS No.:1021839-18-8
Molecular Formula:C₃₀H₃₃Mo₃O₇P
Molecular Weight:824.382
Hs Code.:

Synonyms:[Mo3(η5-cyclopentadienyl)2(μ3-methylidyne)(μ-dicyclohexylphosphide)(CO)7]

Suppliers and Price of [Mo3(η5-cyclopentadienyl)2(μ3-methylidyne)(μ-dicyclohexylphosphide)(CO)7]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Mo3(η5-cyclopentadienyl)2(μ3-methylidyne)(μ-dicyclohexylphosphide)(CO)7]

Chemical Property:

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Technology Process of [Mo3(η5-cyclopentadienyl)2(μ3-methylidyne)(μ-dicyclohexylphosphide)(CO)7]

There total 2 articles about [Mo3(η5-cyclopentadienyl)2(μ3-methylidyne)(μ-dicyclohexylphosphide)(CO)7] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: [Mo2(η5-cyclopentadienyl)2(μ-CH3)(μ-dicyclohexylphosphide)(CO)2]

: 13939-06-5,199620-15-0
molybdenum hexacarbonyl

: 1021839-18-8
[Mo3(η5-cyclopentadienyl)2(μ3-methylidyne)(μ-dicyclohexylphosphide)(CO)7]

Guidance literature:: In toluene; byproducts: H2; Irradiation (UV/VIS); (N2); using Schlenk techniques; irradn. of toluene soln. of Mo2Cp2(μ-CH3)(μ-PCy2)(CO)2 and Mo(CO)6 for 5 h; removal of solvent under vac., dissolving in min. CH2Cl2; chromy. through alumina (activity IV) at 288 K; elution with CH2Cl2-petroleum ether (1:8); removal of solvent under vac., elem. anal.;
DOI:10.1021/om900961u

Reference yield:

: 537683-55-9
[((η⁵-cyclopentadienyl)molybdenum(carbonyl))2(μ-methyl)(μ-dicyclohexylphosphido)]

: 13939-06-5,199620-15-0
molybdenum hexacarbonyl

: 1021839-18-8
[Mo3(η5-cyclopentadienyl)2(μ3-methylidyne)(μ-dicyclohexylphosphide)(CO)7]

Guidance literature:: In not given; byproducts: H2; Irradiation (UV/VIS);
DOI:10.1021/om800061z

Reference yield: 75.0%

: 1021839-18-8
[Mo3(η5-cyclopentadienyl)2(μ3-methylidyne)(μ-dicyclohexylphosphide)(CO)7]

: 201230-82-2
carbon monoxide

: [Mo2(η5-cyclopentadienyl)2(μ-ketenyl)(μ-dicyclohexylphosphide)(CO)2]

: 13939-06-5,199620-15-0
molybdenum hexacarbonyl

Guidance literature:: In toluene; High Pressure; under N2; toluene soln. of Mo complex cooled to 77 K; evacuated under vac.; CO introduced; closed; warmed to room temp.; stirred at 333 K for 2.5 d; solvent removed under vac.; washed with petroleum ether; elem. anal.;
DOI:10.1021/om1011819