N⁶,N⁶-dibenzoyl-5'-deoxy-2',3'-O-isopropylidene-5',5'-(N,N'-diphenylethylenediamino)adenosine

Base Information

• Chemical Name: N⁶,N⁶-dibenzoyl-5'-deoxy-2',3'-O-isopropylidene-5',5'-(N,N'-diphenylethylenediamino)adenosine
• CAS No.: 119244-46-1
• Molecular Formula: C₄₁H₃₇N₇O₅
• Molecular Weight: 707.789

Synonyms:N⁶,N⁶-dibenzoyl-5'-deoxy-2',3'-O-isopropylidene-5',5'-(N,N'-diphenylethylenediamino)adenosine

Chemical Property of N⁶,N⁶-dibenzoyl-5'-deoxy-2',3'-O-isopropylidene-5',5'-(N,N'-diphenylethylenediamino)adenosine

Chemical Property:

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Technology Process of N⁶,N⁶-dibenzoyl-5'-deoxy-2',3'-O-isopropylidene-5',5'-(N,N'-diphenylethylenediamino)adenosine

There total 1 articles about N⁶,N⁶-dibenzoyl-5'-deoxy-2',3'-O-isopropylidene-5',5'-(N,N'-diphenylethylenediamino)adenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

N6-benzoyl-5'-deoxy-2',3'-O-isopropylidiene-5',5'-(N,N'-diphenylethylenediamino)adenosine (43077-03-8) + benzoyl chloride (98-88-4) → N6,N6-dibenzoyl-5'-deoxy-2',3'-O-isopropylidene-5',5'-(N,N'-diphenylethylenediamino)adenosine (119244-46-1)

Guidance literature:

With pyridine; Ambient temperature;

DOI:10.1021/jm00106a028

Reference yield:

N6,N6-dibenzoyl-5'-deoxy-2',3'-O-isopropylidene-5',5'-(N,N'-diphenylethylenediamino)adenosine (119244-46-1) → N6,N6-bis-benzoyl-2',3'-O-isopropylideneadenosine-5'-aldehyde (119244-47-2)

Guidance literature:

With toluene-4-sulfonic acid; In dichloromethane; acetone; for 1.5h; Yield given;

DOI:10.1021/jm00106a028

Reference yield:

N6,N6-dibenzoyl-5'-deoxy-2',3'-O-isopropylidene-5',5'-(N,N'-diphenylethylenediamino)adenosine (119244-46-1) → N6,N6-dibenzoyl-5'deoxy-5',5'-difluoro-2',3'-O-isopropylideneadenosine (119244-34-7)

Guidance literature:

Multi-step reaction with 2 steps

1: p-toluenesulfonic acid monohydrate / CH₂Cl₂; acetone / 1.5 h

2: 18 percent / (diethylamido)sulfur trifluoride / CH₂Cl₂ / 6 h

With (diethylamido)sulfur trifluoride; toluene-4-sulfonic acid; In dichloromethane; acetone;

DOI:10.1021/jm00106a028

upstream raw materials:

N⁶-benzoyl-5'-deoxy-2',3'-O-isopropylidiene-5',5'-(N,N'-diphenylethylenediamino)adenosine

benzoyl chloride

Downstream raw materials:

N⁶,N⁶-bis-benzoyl-2',3'-O-isopropylideneadenosine-5'-aldehyde

5'-deoxy-5',5'-difluoroadenosine

N⁶,N⁶-dibenzoyl-5'deoxy-5',5'-difluoro-2',3'-O-isopropylideneadenosine

N-(9-{(3aR,4R,6aS)-6-[1-Fluoro-meth-(E)-ylidene]-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl}-9H-purin-6-yl)-benzamide

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