4-Methoxy-benzoic acid [2-[(Z)-hydroxyimino]-1-methyl-prop-(Z)-ylidene]-hydrazide

Base Information

Chemical Name:4-Methoxy-benzoic acid [2-[(Z)-hydroxyimino]-1-methyl-prop-(Z)-ylidene]-hydrazide
CAS No.:122081-19-0
Molecular Formula:C₁₂H₁₅N₃O₃
Molecular Weight:249.269
Hs Code.:

Synonyms:4-Methoxy-benzoic acid [2-[(Z)-hydroxyimino]-1-methyl-prop-(Z)-ylidene]-hydrazide

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Chemical Property of 4-Methoxy-benzoic acid [2-[(Z)-hydroxyimino]-1-methyl-prop-(Z)-ylidene]-hydrazide

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Technology Process of 4-Methoxy-benzoic acid [2-[(Z)-hydroxyimino]-1-methyl-prop-(Z)-ylidene]-hydrazide

There total 1 articles about 4-Methoxy-benzoic acid [2-[(Z)-hydroxyimino]-1-methyl-prop-(Z)-ylidene]-hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3290-99-1
4-methoxybenzoic acid hydrazide

: 135636-66-7
butane-2,3-dione mono-oxime

: 122081-19-0
4-Methoxy-benzoic acid [2-[(Z)-hydroxyimino]-1-methyl-prop-(Z)-ylidene]-hydrazide

Guidance literature:: In methanol; Yield given; Ambient temperature;
DOI:10.1039/P19890000619

Reference yield: 80.0%

: 1291-32-3
zirconocene dichloride

: 122081-19-0
diacetylmonoxime 4-methoxybenzoyl hydrazone

: {zirconium(η5-cyclopentadienyl)(OCH3C6H4C(O)NNC(CH3)C(CH3)NO)Cl}

Guidance literature:: In tetrahydrofuran; toluene; byproducts: N(C2H5)3*HCl; stirring equimolar amt. of Zr complex and ligand in THF/toluene at room temp. for 6-7 h, presence of N(C2H5)3, under N2;; filtration; evapn. of solvent under reduced pressure; filtration; washing; recrystn. from THF/petroleum ether; drying in vac.; elem. anal.;;

Reference yield: 70.0%

: 1271-19-8
bis(cyclopentadienyl)titanium dichloride

: 122081-19-0
diacetylmonoxime 4-methoxybenzoyl hydrazone

: {titanium(η5-cyclopentadienyl)(OCH3C6H4C(O)NNC(CH3)C(CH3)NO)Cl}

Guidance literature:: In tetrahydrofuran; toluene; byproducts: N(C2H5)3*HCl; stirring equimolar amt. of Ti complex and ligand in THF/toluene at room temp. for 6-7 h, presence of N(C2H5)3, under N2;; filtration; evapn. of solvent under reduced pressure; filtration; washing; recrystn. from THF/petroleum ether; drying in vac.; elem. anal.;;