4-Methoxy-benzoic acid 4,5-dimethyl-[1,2,3]triazol-1-yl ester

Base Information

• Chemical Name: 4-Methoxy-benzoic acid 4,5-dimethyl-[1,2,3]triazol-1-yl ester
• CAS No.: 122081-23-6
• Molecular Formula: C₁₂H₁₃N₃O₃
• Molecular Weight: 247.254
• Mol file: 122081-23-6.mol

Synonyms:4-Methoxy-benzoic acid 4,5-dimethyl-[1,2,3]triazol-1-yl ester

Chemical Property of 4-Methoxy-benzoic acid 4,5-dimethyl-[1,2,3]triazol-1-yl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-Methoxy-benzoic acid 4,5-dimethyl-[1,2,3]triazol-1-yl ester

There total 3 articles about 4-Methoxy-benzoic acid 4,5-dimethyl-[1,2,3]triazol-1-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

4-Methoxy-benzoic acid [2-[(Z)-hydroxyimino]-1-methyl-prop-(Z)-ylidene]-hydrazide (122081-19-0) → 4-Methoxy-benzoic acid 4,5-dimethyl-[1,2,3]triazol-1-yl ester (122081-23-6)

Guidance literature:

With lead(IV) acetate; In dichloromethane; acetic acid; at 0 ℃; for 0.5h;

DOI:10.1039/P19890000619

Reference yield: 23.0%

4-Methoxy-benzoic acid [2-[(Z)-hydroxyimino]-1-methyl-prop-(Z)-ylidene]-hydrazide (122081-19-0) → C12H13NO4 (24561-40-8) + 4-Methoxy-benzoic acid 4,5-dimethyl-[1,2,3]triazol-1-yl ester (122081-23-6) + C20H21N3O5 (122081-28-1) + 4-methoxybenzoic acid (100-09-4)

Guidance literature:

With lead(IV) acetate; In dichloromethane; at 0 ℃; Yield given;

DOI:10.1039/P19890000619

Reference yield:

4-methoxybenzoic acid hydrazide (3290-99-1) → 4-Methoxy-benzoic acid 4,5-dimethyl-[1,2,3]triazol-1-yl ester (122081-23-6)

Guidance literature:

Multi-step reaction with 2 steps

1: methanol / Ambient temperature

2: 48 percent / lead tetra-acetate / CH₂Cl₂; acetic acid / 0.5 h / 0 °C

With lead(IV) acetate; In methanol; dichloromethane; acetic acid;

DOI:10.1039/P19890000619

upstream raw materials:

4-Methoxy-benzoic acid [2-[(Z)-hydroxyimino]-1-methyl-prop-(Z)-ylidene]-hydrazide

4-methoxybenzoic acid hydrazide

Downstream raw materials:

C₂₀H₂₁N₃O₅

N-(4-chlorophenyl)-4-methoxybenzamide

4,5-dimethyl-1,2,3-triazol-1-ol

4-methoxy-N-phenylbenzamide