ethyl O-benzylnitroethanol

Base Information

Chemical Name:ethyl O-benzylnitroethanol
CAS No.:118577-16-5
Molecular Formula:C₈H₉NO₃
Molecular Weight:167.164
Hs Code.:

Synonyms:ethyl O-benzylnitroethanol

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Chemical Property of ethyl O-benzylnitroethanol

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Technology Process of ethyl O-benzylnitroethanol

There total 1 articles about ethyl O-benzylnitroethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 3587-60-8
Benzyloxymethyl chloride

: 118577-16-5
ethyl O-benzylnitroethanol

Guidance literature:: With silver(I) nitrite; In tetrahydrofuran; toluene; 1.) -25 deg C, 1 h, 2.) 0 deg C, 1 h;
DOI:10.1021/jo00265a054

Reference yield: 65.0%

: 118577-16-5
ethyl O-benzylnitroethanol

: 295365-33-2
ethyl tert-butoxycarbonylamino(toluene-4-sulfonyl)acetate

: ethyl (Z)-α-N-t-butoxycarbonyl-β-O-benzyl-α,β-didehydroserinate

Guidance literature:: ethyl O-benzylnitroethanol; With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 0.166667h;

ethyl tert-butoxycarbonylamino(toluene-4-sulfonyl)acetate; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at -40 - 20 ℃;
DOI:10.1246/bcsj.73.1605

Reference yield: 63.0%

: 118577-16-5
ethyl O-benzylnitroethanol

: 295365-34-3
ethyl benzyloxycarbonylamino(toluene-4-sulfonyl)acetate

: ethyl (Z)-α-N-benzyloxycarbonyl-β-O-benzyl-α,β-didehydroserinate

Guidance literature:: ethyl O-benzylnitroethanol; With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 0.166667h;

ethyl benzyloxycarbonylamino(toluene-4-sulfonyl)acetate; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at -40 - 20 ℃;
DOI:10.1246/bcsj.73.1605