Technology Process of C14H15F3N4
There total 6 articles about C14H15F3N4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
methanol; isopropyl alcohol;
at 50 ℃;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / N,N-dimethyl-formamide / 0.17 h / 150 °C / Microwave irradiation
2: tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 0.17 h / 150 °C / Microwave irradiation
3: palladium 10% on activated carbon; hydrogen / methanol; isopropyl alcohol / 50 °C / Inert atmosphere
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium(0); palladium 10% on activated carbon; hydrogen; potassium acetate;
In
methanol; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; isopropyl alcohol;
2: |Suzuki Coupling;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 0.17 h / 150 °C / Microwave irradiation
2: palladium 10% on activated carbon; hydrogen / methanol; isopropyl alcohol / 50 °C / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); palladium 10% on activated carbon; hydrogen;
In
methanol; 1,2-dimethoxyethane; water; isopropyl alcohol;
1: |Suzuki Coupling;