Technology Process of 6-benzenesulfonyl-hexa-2,4-dienoic acid hydroxamide
There total 6 articles about 6-benzenesulfonyl-hexa-2,4-dienoic acid hydroxamide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydroxylamine;
In
tetrahydrofuran; dichloromethane; water;
at 20 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C
2: hydroxylamine / tetrahydrofuran; dichloromethane; water / 1 h / 20 °C
With
oxalyl dichloride; hydroxylamine;
N,N-dimethyl-formamide;
In
tetrahydrofuran; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetra-(n-butyl)ammonium iodide / tetrahydrofuran / 2 h / Heating / reflux
2: sodium hydroxide; water / methanol / 1 h / Heating / reflux
3: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C
4: hydroxylamine / tetrahydrofuran; dichloromethane; water / 1 h / 20 °C
With
sodium hydroxide; oxalyl dichloride; water; hydroxylamine; tetra-(n-butyl)ammonium iodide;
N,N-dimethyl-formamide;
In
tetrahydrofuran; methanol; dichloromethane; water;
