[2,6-bis(methoxymethyl)phenyl]diphenyltin chloride

Base Information

Chemical Name:[2,6-bis(methoxymethyl)phenyl]diphenyltin chloride
CAS No.:770743-92-5
Molecular Formula:C₂₂H₂₃ClO₂Sn
Molecular Weight:473.586
Hs Code.:

Synonyms:[2,6-bis(methoxymethyl)phenyl]diphenyltin chloride

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Chemical Property of [2,6-bis(methoxymethyl)phenyl]diphenyltin chloride

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Technology Process of [2,6-bis(methoxymethyl)phenyl]diphenyltin chloride

There total 1 articles about [2,6-bis(methoxymethyl)phenyl]diphenyltin chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 65654-53-7
1-bromo-2,6-bis(methoxymethyl)benzene

: 1135-99-5
diphenyltin(IV) dichloride

: 770743-92-5
[2,6-bis(methoxymethyl)phenyl]diphenyltin chloride

Guidance literature:: With nBuLi; In diethyl ether; hexane; nBuLi was added to stirred soln. of ligand in Et2O at -78°C, stirred for 2 h, added dropwise to hexane soln. of Sn-compound at -78°C, stirred for 2 h under Ar; solvent was evapd. in vacuo, dissolved in CHCl3, filtered, concd., layered with pentane, crystd.; elem. anal.;
DOI:10.1021/om020361i

Reference yield: 94.0%

: 770743-92-5
[2,6-bis(methoxymethyl)phenyl]diphenyltin chloride

: Ag[1-CB₁₁H₁₂]*1.5C₆H₆

: [1-(2,6-(MeOCH₂)2C₆H₃)SnPh₂]2[Ag(1-CB₁₁H₁₂)3]

Guidance literature:: In dichloromethane; byproducts: AgCl; (Ar); std. Schlenk technique; light protected; soln. of Sn compd. (2 equiv.) in CH2Cl2 was stirred with Ag compd. (3 equiv.) for 2 h; filtered; filtrate evapd.; washed (pentane); elem. anal.;
DOI:10.1021/om060516c

Reference yield: 86.0%

: 770743-92-5
[2,6-bis(methoxymethyl)phenyl]diphenyltin chloride

: Ag[1-CB₁₁H₁₂]*1.5C₆H₆

: [1-(2,6-(MeOCH₂)2C₆H₃)SnPh₂][1-CB₁₁H₁₂]

Guidance literature:: In tetrahydrofuran; byproducts: AgCl; (Ar); std. Schlenk technique; light protected; soln. of Sn compd. (1 equiv.) in THF was stirred with Ag compd. (1 equiv.) for 1 d; filtered; filtrate evapd.; washed (pentane); elem. anal.;
DOI:10.1021/om060516c