Acetic acid (S)-2-((1S,2S)-2-amino-1-ethyl-3-phenyl-propylamino)-3-methyl-butyl ester

Base Information

• Chemical Name: Acetic acid (S)-2-((1S,2S)-2-amino-1-ethyl-3-phenyl-propylamino)-3-methyl-butyl ester
• CAS No.: 123054-03-5
• Molecular Formula: C₁₈H₃₀N₂O₂
• Molecular Weight: 306.448

Synonyms:Acetic acid (S)-2-((1S,2S)-2-amino-1-ethyl-3-phenyl-propylamino)-3-methyl-butyl ester

Chemical Property of Acetic acid (S)-2-((1S,2S)-2-amino-1-ethyl-3-phenyl-propylamino)-3-methyl-butyl ester

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Technology Process of Acetic acid (S)-2-((1S,2S)-2-amino-1-ethyl-3-phenyl-propylamino)-3-methyl-butyl ester

There total 18 articles about Acetic acid (S)-2-((1S,2S)-2-amino-1-ethyl-3-phenyl-propylamino)-3-methyl-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

Acetic acid (S)-2-[benzyl-((1S,2S)-2-dibenzylamino-1-ethyl-3-phenyl-propyl)-amino]-3-methyl-butyl ester (123054-02-4) → Acetic acid (S)-2-((1S,2S)-2-amino-1-ethyl-3-phenyl-propylamino)-3-methyl-butyl ester (123054-03-5)

Guidance literature:

With hydrogen; palladium dihydroxide; In ethyl acetate; for 48h; under 3040 Torr; Ambient temperature;

DOI:10.1021/jo00284a032

Reference yield:

Acetic acid (S)-2-[benzyl-((1R,2S)-2-dibenzylamino-1-ethyl-3-phenyl-propyl)-amino]-3-methyl-butyl ester (123054-02-4) → Acetic acid (S)-2-((1R,2S)-2-amino-1-ethyl-3-phenyl-propylamino)-3-methyl-butyl ester (123054-03-5)

Guidance literature:

With hydrogen; palladium dihydroxide; In ethyl acetate; for 48h; under 3040 Torr; Ambient temperature;

DOI:10.1021/jo00284a032

Reference yield:

Acetic acid (S)-2-[benzyl-((1R,2R)-2-dibenzylamino-1-ethyl-3-phenyl-propyl)-amino]-3-methyl-butyl ester (123054-02-4) → Acetic acid (S)-2-((1R,2R)-2-amino-1-ethyl-3-phenyl-propylamino)-3-methyl-butyl ester (123054-03-5)

Guidance literature:

With hydrogen; palladium dihydroxide; In ethyl acetate; for 48h; under 3040 Torr; Ambient temperature;

DOI:10.1021/jo00284a032

upstream raw materials:

Acetic acid (S)-2-[benzyl-((1R,2R)-2-dibenzylamino-1-ethyl-3-phenyl-propyl)-amino]-3-methyl-butyl ester

(S)-valinol

N,N-dibenzyl-(R)-2-amino-3-phenylpropanal

N-benzyl-L-valinol

Downstream raw materials:

(1'S,4S,5S)-1-<1'-(acetoxymethyl)-2'-methylpropyl>-4-benzyl-5-ethyl-2-imidazolidone

(1'S,4S,5R)-1-<1'-(acetoxymethyl)-2'-methylpropyl>-4-benzyl-5-ethyl-2-imidazolidone

(1'S,2R,3R)-N²,N²,N³-tribenzyl-N³-<1'-(hydroxymethyl)-2'-methylpropyl>-1-phenyl-2,3-pentanediamine

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