1,1-dimethylethyl 3-{[2-(4-biphenylyl)-1H-imidazo[4,5-c]pyridin-1-yl]methyl}-1-pyrrolidinecarboxylate

Base Information

Chemical Name:1,1-dimethylethyl 3-{[2-(4-biphenylyl)-1H-imidazo[4,5-c]pyridin-1-yl]methyl}-1-pyrrolidinecarboxylate
CAS No.:1309806-07-2
Molecular Formula:C₂₈H₃₀N₄O₂
Molecular Weight:454.572
Hs Code.:

Synonyms:1,1-dimethylethyl 3-{[2-(4-biphenylyl)-1H-imidazo[4,5-c]pyridin-1-yl]methyl}-1-pyrrolidinecarboxylate

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Chemical Property of 1,1-dimethylethyl 3-{[2-(4-biphenylyl)-1H-imidazo[4,5-c]pyridin-1-yl]methyl}-1-pyrrolidinecarboxylate

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Technology Process of 1,1-dimethylethyl 3-{[2-(4-biphenylyl)-1H-imidazo[4,5-c]pyridin-1-yl]methyl}-1-pyrrolidinecarboxylate

There total 6 articles about 1,1-dimethylethyl 3-{[2-(4-biphenylyl)-1H-imidazo[4,5-c]pyridin-1-yl]methyl}-1-pyrrolidinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₈H₃₂N₄O₂

: 1309806-07-2
1,1-dimethylethyl 3-{[2-(4-biphenylyl)-1H-imidazo[4,5-c]pyridin-1-yl]methyl}-1-pyrrolidinecarboxylate

Guidance literature:: palladium 10% on activated carbon; In butan-1-ol; at 85 ℃; for 3h; Product distribution / selectivity;

Reference yield:

: 1309806-06-1
1,1-dimethylethyl 3-{[(3-nitro-4-pyridinyl)amino]methyl}-1-pyrrolidinecarboxylate

: 3218-36-8
4-Phenylbenzaldehyde

: 1309806-07-2
1,1-dimethylethyl 3-{[2-(4-biphenylyl)-1H-imidazo[4,5-c]pyridin-1-yl]methyl}-1-pyrrolidinecarboxylate

Guidance literature:: 1,1-dimethylethyl 3-{[(3-nitro-4-pyridinyl)amino]methyl}-1-pyrrolidinecarboxylate; 4-Phenylbenzaldehyde; With sodium dithionite; In ethanol; water; at 70 ℃; for 120h;

With ammonium hydroxide; In water; ethyl acetate; Product distribution / selectivity;

Reference yield:

: 13091-23-1
4-chloro-3-nitropyridine

: 1309806-07-2
1,1-dimethylethyl 3-{[2-(4-biphenylyl)-1H-imidazo[4,5-c]pyridin-1-yl]methyl}-1-pyrrolidinecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / ethanol / 2 h / 70 °C / Inert atmosphere

2: sodium dithionite / ethanol; water / 120 h / 70 °C

With sodium dithionite; triethylamine; In ethanol; water;