C₃₀H₅₀O₉Si

Base Information

Chemical Name:C₃₀H₅₀O₉Si
CAS No.:1392829-12-7
Molecular Formula:C₃₀H₅₀O₉Si
Molecular Weight:582.807
Hs Code.:

C<sub>30</sub>H<sub>50</sub>O<sub>9</sub>Si

Synonyms:C₃₀H₅₀O₉Si

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Chemical Property of C₃₀H₅₀O₉Si

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Technology Process of C₃₀H₅₀O₉Si

There total 18 articles about C₃₀H₅₀O₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1392829-11-6
C₃₃H₅₆O₈S₂Si

: 1392829-12-7
C₃₀H₅₀O₉Si

Guidance literature:: With 2,6-dimethylpyridine; isothiocyanic acid; silver nitrate; In water; acetonitrile; at 0 ℃; for 0.05h; Inert atmosphere;
DOI:10.1002/chem.201503880

Reference yield:

: C₂₀H₃₀O₅Si

: 1392829-12-7
C₃₀H₅₀O₉Si

Guidance literature:: Multi-step reaction with 12 steps

1.1: boron trifluoride diethyl etherate / diethyl ether / 0 °C

2.1: sodium periodate; ruthenium trichloride; water; zinc(II) chloride / ethyl acetate; acetonitrile / 0 °C

3.1: toluene-4-sulfonic acid / tetrahydrofuran / 40 °C

4.1: sodium tetrahydroborate / methanol; dichloromethane / 0 °C

5.1: sodium hydride / tetrahydrofuran / 0 °C

5.2: 0 - 20 °C

6.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / benzene / 80 °C

7.1: LiDBB / tetrahydrofuran / -78 °C

8.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 0 - 20 °C

9.1: n-butyllithium / tetrahydrofuran / 20 °C

9.2: -78 - 0 °C

10.1: pyridine; Dess-Martin periodane / dichloromethane / 0 - 20 °C

11.1: diisobutylaluminium hydride / dichloromethane / -78 °C

12.1: N-chloro-succinimide; water; silver nitrate / acetonitrile / 20 °C

With pyridine; ruthenium trichloride; sodium tetrahydroborate; sodium periodate; N-chloro-succinimide; n-butyllithium; 2,2'-azobis(isobutyronitrile); boron trifluoride diethyl etherate; water; tri-n-butyl-tin hydride; sulfur trioxide pyridine complex; sodium hydride; diisobutylaluminium hydride; Dess-Martin periodane; toluene-4-sulfonic acid; silver nitrate; dimethyl sulfoxide; triethylamine; zinc(II) chloride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; ethyl acetate; acetonitrile; benzene; 6.1: Barton-McCombie deoxygenation / 8.1: Parikh-Doering oxidation;
DOI:10.1016/j.tetlet.2012.06.005

Reference yield:

: 1392829-16-1
C₂₄H₃₈O₇Si

: 1392829-12-7
C₃₀H₅₀O₉Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium tetrahydroborate / methanol; dichloromethane / 0 °C

2.1: sodium hydride / tetrahydrofuran / 0 °C

2.2: 0 - 20 °C

3.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / benzene / 80 °C

4.1: LiDBB / tetrahydrofuran / -78 °C

5.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 0 - 20 °C

6.1: n-butyllithium / tetrahydrofuran / 20 °C

6.2: -78 - 0 °C

7.1: pyridine; Dess-Martin periodane / dichloromethane / 0 - 20 °C

8.1: diisobutylaluminium hydride / dichloromethane / -78 °C

9.1: N-chloro-succinimide; water; silver nitrate / acetonitrile / 20 °C

With pyridine; sodium tetrahydroborate; N-chloro-succinimide; n-butyllithium; 2,2'-azobis(isobutyronitrile); water; tri-n-butyl-tin hydride; sulfur trioxide pyridine complex; sodium hydride; diisobutylaluminium hydride; Dess-Martin periodane; silver nitrate; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; methanol; dichloromethane; acetonitrile; benzene; 3.1: Barton-McCombie deoxygenation / 5.1: Parikh-Doering oxidation;
DOI:10.1016/j.tetlet.2012.06.005