8-<3,5-Bis<2,6-bis(methoxymethoxy)-3,5-diphenylphenyl>phenyl>-2-methylquinoline

Base Information

Chemical Name:8-<3,5-Bis<2,6-bis(methoxymethoxy)-3,5-diphenylphenyl>phenyl>-2-methylquinoline
CAS No.:142841-82-5
Molecular Formula:C₆₀H₅₃NO₈
Molecular Weight:916.083
Hs Code.:

Synonyms:8-<3,5-Bis<2,6-bis(methoxymethoxy)-3,5-diphenylphenyl>phenyl>-2-methylquinoline

Suppliers and Price of 8-<3,5-Bis<2,6-bis(methoxymethoxy)-3,5-diphenylphenyl>phenyl>-2-methylquinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-<3,5-Bis<2,6-bis(methoxymethoxy)-3,5-diphenylphenyl>phenyl>-2-methylquinoline

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Technology Process of 8-<3,5-Bis<2,6-bis(methoxymethoxy)-3,5-diphenylphenyl>phenyl>-2-methylquinoline

There total 3 articles about 8-<3,5-Bis<2,6-bis(methoxymethoxy)-3,5-diphenylphenyl>phenyl>-2-methylquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61047-43-6
8-bromo-2-methylquinoline

: 142841-82-5
8-<3,5-Bis<2,6-bis(methoxymethoxy)-3,5-diphenylphenyl>phenyl>-2-methylquinoline

Guidance literature:: Multi-step reaction with 2 steps

2: 1.) n-BuLi, ZnCl₂ / 2.) NiCl₂(PPh₃)2 / 1.) Et₂O, hexane, 0 deg C, 1 h, r.t., 1 h then THF, r.t., 1 h, 2.) reflux, 17 h

With n-butyllithium; zinc(II) chloride; bis(triphenylphosphine)nickel(II) chloride;
DOI:10.1021/jo00076a031

Reference yield:

: 626-39-1
1,3,5-trisbromobenzene

: 142841-82-5
8-<3,5-Bis<2,6-bis(methoxymethoxy)-3,5-diphenylphenyl>phenyl>-2-methylquinoline

Guidance literature:: Multi-step reaction with 2 steps

2: 1.) n-BuLi, ZnCl₂ / 2.) NiCl₂(PPh₃)2 / 1.) Et₂O, hexane, 0 deg C, 1 h, r.t., 1 h then THF, r.t., 1 h, 2.) reflux, 17 h

With n-butyllithium; zinc(II) chloride; bis(triphenylphosphine)nickel(II) chloride;
DOI:10.1021/jo00076a031

Reference yield:

: 142841-81-4
8-(3,5-Dibromophenyl)-2-methylquinoline

: 142841-79-0
4',6'-Bis(methoxymethoxy)-m-terphenyl

: 142841-82-5
8-<3,5-Bis<2,6-bis(methoxymethoxy)-3,5-diphenylphenyl>phenyl>-2-methylquinoline

Guidance literature:: With n-butyllithium; zinc(II) chloride; bis(triphenylphosphine)nickel(II) chloride; Yield given. Multistep reaction; 1.) Et₂O, hexane, 0 deg C, 1 h, r.t., 1 h then THF, r.t., 1 h, 2.) reflux, 17 h;
DOI:10.1021/jo00076a031