Methyl 3-(tert-butylcarbamoyl)benzoate

Base Information

Chemical Name:Methyl 3-(tert-butylcarbamoyl)benzoate
CAS No.:67852-99-7
Molecular Formula:C₁₃H₁₇NO₃
Molecular Weight:235.283
Hs Code.:
DSSTox Substance ID:DTXSID401213557

Synonyms:methyl 3-(tert-butylcarbamoyl)benzoate;67852-99-7;Methyl 3-[[(1,1-dimethylethyl)amino]carbonyl]benzoate;SCHEMBL4725130;DTXSID401213557;methyl3-(tert-butylcarbamoyl)benzoate;BS-29409;DB-158369

Suppliers and Price of Methyl 3-(tert-butylcarbamoyl)benzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Methyl 3-(tert-butylcarbamoyl)benzoate

Chemical Property:

XLogP3:2.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:235.12084340
Heavy Atom Count:17
Complexity:294

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)(C)NC(=O)C1=CC(=CC=C1)C(=O)OC

Technology Process of Methyl 3-(tert-butylcarbamoyl)benzoate

There total 2 articles about Methyl 3-(tert-butylcarbamoyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3441-03-0
3-(methoxycarbonyl)benzoyl chloride

: 75-64-9
tert-butylamine

: 67852-99-7
methyl 3-(tert-butylcarbamoyl)benzoate

Guidance literature:: 3-(methoxycarbonyl)benzoyl chloride; With triethylamine; In diethyl ether; at 0 ℃; for 0.25h;

tert-butylamine; In diethyl ether; at 20 ℃; for 3h;
DOI:10.1021/acs.joc.6b02516

Reference yield:

: 67852-99-7
methyl 3-(tert-butylcarbamoyl)benzoate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield: 80.0%

: 67852-99-7
methyl 3-(tert-butylcarbamoyl)benzoate

: 501-65-5
diphenyl acetylene

: (E)-methyl 3-(tert-butylcarbamoyl)-4-(1,2-diphenylvinyl)benzoate

Guidance literature:: With silver tetrafluoroborate; carbonyl(pentamethylcyclopentadienyl)cobalt diiodide; copper(II) acetate monohydrate; In 1,2-dichloro-ethane; at 100 ℃; for 12h; Sealed tube;
DOI:10.1021/acs.joc.6b02516