4-(4-((benzyl(2-methyl-3-(methylsulfonamido)phenyl)amino)methyl)phenoxy)phenyl 5-((methoxycarbonyl)amino)-2-methylpentanoate

Base Information

Chemical Name:4-(4-((benzyl(2-methyl-3-(methylsulfonamido)phenyl)amino)methyl)phenoxy)phenyl 5-((methoxycarbonyl)amino)-2-methylpentanoate
CAS No.:1567941-39-2
Molecular Formula:C₃₆H₄₁N₃O₇S
Molecular Weight:659.803
Hs Code.:

Synonyms:4-(4-((benzyl(2-methyl-3-(methylsulfonamido)phenyl)amino)methyl)phenoxy)phenyl 5-((methoxycarbonyl)amino)-2-methylpentanoate

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Chemical Property of 4-(4-((benzyl(2-methyl-3-(methylsulfonamido)phenyl)amino)methyl)phenoxy)phenyl 5-((methoxycarbonyl)amino)-2-methylpentanoate

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Technology Process of 4-(4-((benzyl(2-methyl-3-(methylsulfonamido)phenyl)amino)methyl)phenoxy)phenyl 5-((methoxycarbonyl)amino)-2-methylpentanoate

There total 5 articles about 4-(4-((benzyl(2-methyl-3-(methylsulfonamido)phenyl)amino)methyl)phenoxy)phenyl 5-((methoxycarbonyl)amino)-2-methylpentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5693-62-9
2,3,4,5-tetrahydro-6-methoxypyridine

: 1567941-39-2
4-(4-((benzyl(2-methyl-3-(methylsulfonamido)phenyl)amino)methyl)phenoxy)phenyl 5-((methoxycarbonyl)amino)-2-methylpentanoate

Guidance literature:: Multi-step reaction with 5 steps

1: tert.-butyl lithium / tetrahydrofuran / 0.25 h / -78 - 0 °C

2: hydrogenchloride / water; chloroform / 20 °C

3: N-ethyl-N,N-diisopropylamine / 2 h / 0 - 20 °C

4: water; tetrahydrofuran / 6 h / Alkaline conditions

5: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 1 h / 20 °C

With hydrogenchloride; dmap; tert.-butyl lithium; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; chloroform; water;
DOI:10.1016/j.bmcl.2013.12.126

Reference yield:

: 1567047-91-9
C₈H₁₅NO₄

: 1567941-37-0
C₂₈H₂₈N₂O₄S

: 1567941-39-2
4-(4-((benzyl(2-methyl-3-(methylsulfonamido)phenyl)amino)methyl)phenoxy)phenyl 5-((methoxycarbonyl)amino)-2-methylpentanoate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1016/j.bmcl.2013.12.126

Reference yield:

: 179685-56-4
1-Aza-2-methoxy-3-methyl-1-cyclohexene

: 1567941-39-2
4-(4-((benzyl(2-methyl-3-(methylsulfonamido)phenyl)amino)methyl)phenoxy)phenyl 5-((methoxycarbonyl)amino)-2-methylpentanoate

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride / water; chloroform / 20 °C

2: N-ethyl-N,N-diisopropylamine / 2 h / 0 - 20 °C

3: water; tetrahydrofuran / 6 h / Alkaline conditions

4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 1 h / 20 °C

With hydrogenchloride; dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; chloroform; water;
DOI:10.1016/j.bmcl.2013.12.126