1-(4-chloro-benzyl)-6,7-dimethoxy-4-oxo-1,4-dihydro-quinoline-3-carbonitrile

Base Information

• Chemical Name: 1-(4-chloro-benzyl)-6,7-dimethoxy-4-oxo-1,4-dihydro-quinoline-3-carbonitrile
• CAS No.: 957137-98-3
• Molecular Formula: C₁₉H₁₅ClN₂O₃
• Molecular Weight: 354.793

Synonyms:1-(4-chloro-benzyl)-6,7-dimethoxy-4-oxo-1,4-dihydro-quinoline-3-carbonitrile

Chemical Property of 1-(4-chloro-benzyl)-6,7-dimethoxy-4-oxo-1,4-dihydro-quinoline-3-carbonitrile

Chemical Property:

Purity/Quality:

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Technology Process of 1-(4-chloro-benzyl)-6,7-dimethoxy-4-oxo-1,4-dihydro-quinoline-3-carbonitrile

There total 1 articles about 1-(4-chloro-benzyl)-6,7-dimethoxy-4-oxo-1,4-dihydro-quinoline-3-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-chlorobenzyl bromide (622-95-7) + 1,4-dihydro-6,7-dimethoxy-4-oxo-quinoline-3-carbonitrile (214470-52-7,50845-31-3) → 1-(4-chloro-benzyl)-6,7-dimethoxy-4-oxo-1,4-dihydro-quinoline-3-carbonitrile (957137-98-3)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 2 - 4h;

Reference yield:

1-(4-chloro-benzyl)-6,7-dimethoxy-4-oxo-1,4-dihydro-quinoline-3-carbonitrile (957137-98-3) → 1-(4-chloro-benzyl)-N-hydroxy-6,7-dimethoxy-4-oxo-1,4-dihydro-quinoline-3-carboxamidine (957138-36-2)

Guidance literature:

With hydroxylamine; In ethanol; Heating / reflux;

Reference yield:

1-(4-chloro-benzyl)-6,7-dimethoxy-4-oxo-1,4-dihydro-quinoline-3-carbonitrile (957137-98-3) → C19H16ClN5O3 (1356183-43-1)

Guidance literature:

With trimethylsilylazide; di(n-butyl)tin oxide; In toluene; at 110 ℃; for 4h;

DOI:10.1016/j.bmcl.2011.11.013

upstream raw materials:

4-chlorobenzyl bromide

1,4-dihydro-6,7-dimethoxy-4-oxo-quinoline-3-carbonitrile

Downstream raw materials:

1-(4-chloro-benzyl)-N-hydroxy-6,7-dimethoxy-4-oxo-1,4-dihydro-quinoline-3-carboxamidine

C₁₉H₁₆ClN₅O₃

C₁₉H₁₈ClN₃O₄

C₂₆H₂₂ClN₅O₃

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