Technology Process of 6-(4-methoxy-2,5-dimethyl-3,6-dioxocyclohexa-1,4-dienyl)hexyl nitrate
There total 6 articles about 6-(4-methoxy-2,5-dimethyl-3,6-dioxocyclohexa-1,4-dienyl)hexyl nitrate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dipotassium peroxodisulfate; silver nitrate;
In
water; acetonitrile;
at 75 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: silver nitrate / acetonitrile / 0.37 h / 120 °C / Microwave irradiation
2.1: lithium hydroxide / 4 °C
2.2: pH 1
3.1: silver nitrate; dipotassium peroxodisulfate / acetonitrile; water / 3 h / 75 °C
With
dipotassium peroxodisulfate; silver nitrate; lithium hydroxide;
In
water; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: boron trifluoride diethyl etherate / 40 °C
2: sodium hydroxide / methanol / 23 °C
3: [bis(acetoxy)iodo]benzene
4: silver nitrate; dipotassium peroxodisulfate / acetonitrile; water / 3 h / 75 °C
With
dipotassium peroxodisulfate; [bis(acetoxy)iodo]benzene; boron trifluoride diethyl etherate; silver nitrate; sodium hydroxide;
In
methanol; water; acetonitrile;
