6-deoxy-6-C-(diphenylphosphinyl)-1,2:3,5-di-O-isopropylidene-α-D-glucofuranose

Base Information

Chemical Name:6-deoxy-6-C-(diphenylphosphinyl)-1,2:3,5-di-O-isopropylidene-α-D-glucofuranose
CAS No.:79940-58-2
Molecular Formula:C₂₄H₂₉O₆P
Molecular Weight:444.464
Hs Code.:

Synonyms:6-deoxy-6-C-(diphenylphosphinyl)-1,2:3,5-di-O-isopropylidene-α-D-glucofuranose

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Chemical Property of 6-deoxy-6-C-(diphenylphosphinyl)-1,2:3,5-di-O-isopropylidene-α-D-glucofuranose

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Technology Process of 6-deoxy-6-C-(diphenylphosphinyl)-1,2:3,5-di-O-isopropylidene-α-D-glucofuranose

There total 4 articles about 6-deoxy-6-C-(diphenylphosphinyl)-1,2:3,5-di-O-isopropylidene-α-D-glucofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 34322-91-3
1,2:3,5-bis-O-(1-methylethylidene)-6-(p-tolylsulfonyl)-α-D-glucofuranose

: 4559-70-0
Diphenylphosphine oxide

: 79940-58-2
6-deoxy-6-C-(diphenylphosphinyl)-1,2:3,5-di-O-isopropylidene-α-D-glucofuranose

Guidance literature:: With sodium bis(2-methoxyethoxy)aluminium dihydride; In various solvent(s); at 56 ℃; for 10h; Heating;
DOI:10.1016/S0008-6215(00)80984-2

Reference yield:

: 34322-91-3
1,2:3,5-bis-O-(1-methylethylidene)-6-(p-tolylsulfonyl)-α-D-glucofuranose

: 79940-58-2
6-deoxy-6-C-(diphenylphosphinyl)-1,2:3,5-di-O-isopropylidene-α-D-glucofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / sodium dihydrobis(2-methoxyethoxy)aluminate (SDMA) / tetrahydrofuran / 4 h / Heating

2: 38percent aq. H₂O₂ / Ambient temperature

With dihydrogen peroxide; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran;
DOI:10.1246/bcsj.55.2917

Reference yield:

: 829-85-6
diphenylphosphane

: 79940-58-2
6-deoxy-6-C-(diphenylphosphinyl)-1,2:3,5-di-O-isopropylidene-α-D-glucofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / sodium dihydrobis(2-methoxyethoxy)aluminate (SDMA) / tetrahydrofuran / 4 h / Heating

2: 38percent aq. H₂O₂ / Ambient temperature

With dihydrogen peroxide; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran;
DOI:10.1246/bcsj.55.2917