dichloro[dimethylbis(diphenylphosphino)tetrathiafulvalene]platinum(II)

Base Information

Chemical Name:dichloro[dimethylbis(diphenylphosphino)tetrathiafulvalene]platinum(II)
CAS No.:701208-68-6
Molecular Formula:C₃₂H₂₆Cl₂P₂PtS₄
Molecular Weight:866.756
Hs Code.:

Synonyms:dichloro[dimethylbis(diphenylphosphino)tetrathiafulvalene]platinum(II)

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Chemical Property of dichloro[dimethylbis(diphenylphosphino)tetrathiafulvalene]platinum(II)

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Technology Process of dichloro[dimethylbis(diphenylphosphino)tetrathiafulvalene]platinum(II)

There total 2 articles about dichloro[dimethylbis(diphenylphosphino)tetrathiafulvalene]platinum(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 13869-38-0,21264-32-4,13869-42-6
bis(acetonitrile)dichloroplatinum(II)

: 141858-24-4
3,4-bis(diphenylphosphino)-3',4'-dimethyl-2,2',5,5'-tetrathiafulvalene

: 701208-68-6
dichloro[dimethylbis(diphenylphosphino)tetrathiafulvalene]platinum(II)

Guidance literature:: In chloroform; soln. Pt complex and ligand in CHCl3 was refluxed overnight; react. mixt. was cooled to room temp., evapd. in vacuo and washed with Et2O;
DOI:10.1039/b812797b

Reference yield: 70.0%

: 141858-24-4
3,4-bis(diphenylphosphino)-3',4'-dimethyl-2,2',5,5'-tetrathiafulvalene

: 10025-65-7
platinum(II) chloride

: 701208-68-6
dichloro[dimethylbis(diphenylphosphino)tetrathiafulvalene]platinum(II)

Guidance literature:: In chloroform; PtCl2 and ligand were suspended in CHCl3, refluxed overnight under N2; cooled, filtered, cond., Et2O was added, washed with Et2O, dried under vac.; elem. anal.;
DOI:10.1021/ic035447y

Reference yield: 75.0%

: 701208-68-6
dichloro[dimethylbis(diphenylphosphino)tetrathiafulvalene]platinum(II)

: 174091-23-7
Bu₂Sn(1,3-dithiole-2-thione-4,5-dithiolate)

: 1093425-40-1
(3,4-dimethyl-3',4'-bis(diphenylphosphino)tetrathiafulvalene)Pt(4,5-dimercapto-1,3-dithiole-2-thione)

Guidance literature:: In acetone; soln. Pt and Sn complexes in acetone was stirred for 3 h; soln. was evapd. and separated by column chromy. on silica (CHCl3), crystn. from CHCl3-MeOH;
DOI:10.1039/b812797b