2-chloro-3-(methylsulphanyl)-N-(1-methyl-1H-tetrazol-5-yl)-4-(trifluoromethyl)benzamide

Base Information

Chemical Name:2-chloro-3-(methylsulphanyl)-N-(1-methyl-1H-tetrazol-5-yl)-4-(trifluoromethyl)benzamide
CAS No.:1361139-71-0
Molecular Formula:C₁₁H₉ClF₃N₅OS
Molecular Weight:351.74
Hs Code.:

Synonyms:2-chloro-3-(methylsulphanyl)-N-(1-methyl-1H-tetrazol-5-yl)-4-(trifluoromethyl)benzamide

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Chemical Property of 2-chloro-3-(methylsulphanyl)-N-(1-methyl-1H-tetrazol-5-yl)-4-(trifluoromethyl)benzamide

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Technology Process of 2-chloro-3-(methylsulphanyl)-N-(1-methyl-1H-tetrazol-5-yl)-4-(trifluoromethyl)benzamide

There total 3 articles about 2-chloro-3-(methylsulphanyl)-N-(1-methyl-1H-tetrazol-5-yl)-4-(trifluoromethyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 5422-44-6
1-methyl-5-amino-1H-tetrazole

: 2-chloro-4-trifluoromethyl-3-methylsulphanylbenzoic acid

: 1361139-71-0
2-chloro-3-(methylsulphanyl)-N-(1-methyl-1H-tetrazol-5-yl)-4-(trifluoromethyl)benzamide

Guidance literature:: With 1-methyl-1H-imidazole; thionyl chloride; 3-Methylpyridine; In acetonitrile; at 74 ℃; for 6h; Inert atmosphere; Reflux;

Reference yield:

: 54773-19-2
1,2-dichloro-3-(trifluoromethyl)benzene

: 1361139-71-0
2-chloro-3-(methylsulphanyl)-N-(1-methyl-1H-tetrazol-5-yl)-4-(trifluoromethyl)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: tri(butyl)tetradecylphosphonium chloride / water / 6 h / 80 °C / Inert atmosphere

2.1: diisopropylamine; n-butyllithium / tetrahydrofuran; hexane / 5 h / -70 °C / Inert atmosphere

2.2: 2 h / -60 - 23 °C

3.1: 3-Methylpyridine; 1-methyl-1H-imidazole; thionyl chloride / acetonitrile / 6 h / 74 °C / Inert atmosphere; Reflux

With tri(butyl)tetradecylphosphonium chloride; 1-methyl-1H-imidazole; n-butyllithium; thionyl chloride; 3-Methylpyridine; diisopropylamine; In tetrahydrofuran; hexane; water; acetonitrile;