2-(4-(2-(4-chlorophenyl)-2-oxoethoxy)benzylidene)-2,3-dihydro-1H-inden-1-one

Base Information

Chemical Name:2-(4-(2-(4-chlorophenyl)-2-oxoethoxy)benzylidene)-2,3-dihydro-1H-inden-1-one
CAS No.:1631747-96-0
Molecular Formula:C₂₄H₁₇ClO₃
Molecular Weight:388.85
Hs Code.:

Synonyms:2-(4-(2-(4-chlorophenyl)-2-oxoethoxy)benzylidene)-2,3-dihydro-1H-inden-1-one

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Chemical Property of 2-(4-(2-(4-chlorophenyl)-2-oxoethoxy)benzylidene)-2,3-dihydro-1H-inden-1-one

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Technology Process of 2-(4-(2-(4-chlorophenyl)-2-oxoethoxy)benzylidene)-2,3-dihydro-1H-inden-1-one

There total 4 articles about 2-(4-(2-(4-chlorophenyl)-2-oxoethoxy)benzylidene)-2,3-dihydro-1H-inden-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 124996-01-6,92882-99-0
2-(4-hydroxybenzylidene)-2, 3-dihydro-1H-inden-1-one

: 536-38-9
4-chlorobenzoylmethyl bromide

: 1631747-96-0
2-(4-(2-(4-chlorophenyl)-2-oxoethoxy)benzylidene)-2,3-dihydro-1H-inden-1-one

Guidance literature:: With potassium carbonate; In acetone; for 6h; Reflux;
DOI:10.2174/1570180811666140403001212

Reference yield:

: 100-52-7
benzaldehyde

: 1631747-96-0
2-(4-(2-(4-chlorophenyl)-2-oxoethoxy)benzylidene)-2,3-dihydro-1H-inden-1-one

Guidance literature:: Multi-step reaction with 4 steps

1: triethylammonium formate / N,N-dimethyl-formamide / 6 h / 20 °C

2: polyphosphoric acid / 2 h / 20 - 100 °C

3: hydrogenchloride / butan-1-ol; water / 1 h / Reflux

4: potassium carbonate / acetone / 6 h / Reflux

With hydrogenchloride; triethylammonium formate; potassium carbonate; In water; N,N-dimethyl-formamide; acetone; butan-1-ol;
DOI:10.2174/1570180811666140403001212

Reference yield:

: 501-52-0
3-Phenylpropionic acid

: 1631747-96-0
2-(4-(2-(4-chlorophenyl)-2-oxoethoxy)benzylidene)-2,3-dihydro-1H-inden-1-one

Guidance literature:: Multi-step reaction with 3 steps

1: polyphosphoric acid / 2 h / 20 - 100 °C

2: hydrogenchloride / butan-1-ol; water / 1 h / Reflux

3: potassium carbonate / acetone / 6 h / Reflux

With hydrogenchloride; potassium carbonate; In water; acetone; butan-1-ol;
DOI:10.2174/1570180811666140403001212