methyl 3-[({[4-cyano-3-(4-nitrophenyl)isothiazol-5-yl]amino}carbonyl)amino]propanoate

Base Information

Chemical Name:methyl 3-[({[4-cyano-3-(4-nitrophenyl)isothiazol-5-yl]amino}carbonyl)amino]propanoate
CAS No.:1446247-83-1
Molecular Formula:C₁₅H₁₃N₅O₅S
Molecular Weight:375.365
Hs Code.:

Synonyms:methyl 3-[({[4-cyano-3-(4-nitrophenyl)isothiazol-5-yl]amino}carbonyl)amino]propanoate

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Chemical Property of methyl 3-[({[4-cyano-3-(4-nitrophenyl)isothiazol-5-yl]amino}carbonyl)amino]propanoate

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Technology Process of methyl 3-[({[4-cyano-3-(4-nitrophenyl)isothiazol-5-yl]amino}carbonyl)amino]propanoate

There total 6 articles about methyl 3-[({[4-cyano-3-(4-nitrophenyl)isothiazol-5-yl]amino}carbonyl)amino]propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 605661-28-7
5-amino-3-(4-nitrophenyl)isothiazole-4-carbonitrile

: 50835-77-3
2-methoxycarbonylethyl isocyanate

: 1446247-83-1
methyl 3-[({[4-cyano-3-(4-nitrophenyl)isothiazol-5-yl]amino}carbonyl)amino]propanoate

Guidance literature:: 5-amino-3-(4-nitrophenyl)isothiazole-4-carbonitrile; With potassium carbonate; In tetrahydrofuran; dimethyl sulfoxide; at 20 ℃; for 0.25h;

2-methoxycarbonylethyl isocyanate; In tetrahydrofuran; dimethyl sulfoxide; at 20 ℃;

Reference yield:

: 605661-26-5
2-[amino(4-nitrophenyl)methylene]malononitrile

: 1446247-83-1
methyl 3-[({[4-cyano-3-(4-nitrophenyl)isothiazol-5-yl]amino}carbonyl)amino]propanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: O,O-Diethyl hydrogen phosphorodithioate / ethanol; water / 100 °C / Inert atmosphere

2.1: dihydrogen peroxide / ethanol / 22 h / Inert atmosphere

3.1: potassium carbonate / tetrahydrofuran; dimethyl sulfoxide / 0.25 h / 20 °C

3.2: 20 °C

With dihydrogen peroxide; potassium carbonate; O,O-Diethyl hydrogen phosphorodithioate; In tetrahydrofuran; ethanol; water; dimethyl sulfoxide;

Reference yield:

: 909028-96-2
3-amino-3-(4-nitrophenyl)-2-thioformamidoacrylonitrile

: 1446247-83-1
methyl 3-[({[4-cyano-3-(4-nitrophenyl)isothiazol-5-yl]amino}carbonyl)amino]propanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: dihydrogen peroxide / ethanol / 22 h / Inert atmosphere

2.1: potassium carbonate / tetrahydrofuran; dimethyl sulfoxide / 0.25 h / 20 °C

2.2: 20 °C

With dihydrogen peroxide; potassium carbonate; In tetrahydrofuran; ethanol; dimethyl sulfoxide;