N,N''-bis(1-hexylheptyl)-N'-[4-(4'-carboxyphenyl)iminomethylbenzyl]benzo[ghi]perylene-1',2':3,4:9,10-hexacarboxylictris(dicarboximide)

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Chemical Name:N,N''-bis(1-hexylheptyl)-N'-[4-(4'-carboxyphenyl)iminomethylbenzyl]benzo[ghi]perylene-1',2':3,4:9,10-hexacarboxylictris(dicarboximide)
CAS No.:1351949-23-9
Molecular Formula:C₆₉H₇₂N₄O₈
Molecular Weight:1085.35
Hs Code.:

Synonyms:N,N''-bis(1-hexylheptyl)-N'-[4-(4'-carboxyphenyl)iminomethylbenzyl]benzo[ghi]perylene-1',2':3,4:9,10-hexacarboxylictris(dicarboximide)

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Chemical Property of N,N''-bis(1-hexylheptyl)-N'-[4-(4'-carboxyphenyl)iminomethylbenzyl]benzo[ghi]perylene-1',2':3,4:9,10-hexacarboxylictris(dicarboximide)

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Technology Process of N,N''-bis(1-hexylheptyl)-N'-[4-(4'-carboxyphenyl)iminomethylbenzyl]benzo[ghi]perylene-1',2':3,4:9,10-hexacarboxylictris(dicarboximide)

There total 4 articles about N,N''-bis(1-hexylheptyl)-N'-[4-(4'-carboxyphenyl)iminomethylbenzyl]benzo[ghi]perylene-1',2':3,4:9,10-hexacarboxylictris(dicarboximide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1351948-97-4
N,N''-bis(1-hexylheptyl)-N′-(4-formylbenzyl)benzo[ghi]perylene-1′,2′:3,4:9,10-tris(dicarboximide)

: 150-13-0,159246-81-8,8014-65-1
4-amino-benzoic acid

: 1351949-23-9
N,N''-bis(1-hexylheptyl)-N'-[4-(4'-carboxyphenyl)iminomethylbenzyl]benzo[ghi]perylene-1',2':3,4:9,10-hexacarboxylictris(dicarboximide)

Guidance literature:: With magnesium sulfate; In ethanol; Dichlorofluoromethane; at 20 ℃; for 14h; pH=5; Reflux;
DOI:10.1002/chem.201103221

Reference yield:

: 104566-44-1
4-(1,3-dioxacyclopent-2-yl)benzylamine

: 1351949-23-9
N,N''-bis(1-hexylheptyl)-N'-[4-(4'-carboxyphenyl)iminomethylbenzyl]benzo[ghi]perylene-1',2':3,4:9,10-hexacarboxylictris(dicarboximide)

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / quinoline / 12 h / 170 °C

1.2: 12 h / 20 °C

2.1: magnesium sulfate / ethanol; Dichlorofluoromethane / 14 h / 20 °C / pH 5 / Reflux

With hydrogenchloride; magnesium sulfate; In quinoline; ethanol; Dichlorofluoromethane;
DOI:10.1002/chem.201103221

Reference yield:

: 259880-39-2
2,10-bis(1-hexylheptyl)furo[3′,4′:4,5]pyreno-[2,1,10-def:7,8,9-d′e′f ′]diisoquinoline-1,3,5,7,9,11(2H,10H)-hexone

: 1351949-23-9
N,N''-bis(1-hexylheptyl)-N'-[4-(4'-carboxyphenyl)iminomethylbenzyl]benzo[ghi]perylene-1',2':3,4:9,10-hexacarboxylictris(dicarboximide)

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / quinoline / 12 h / 170 °C

1.2: 12 h / 20 °C

2.1: magnesium sulfate / ethanol; Dichlorofluoromethane / 14 h / 20 °C / pH 5 / Reflux

With hydrogenchloride; magnesium sulfate; In quinoline; ethanol; Dichlorofluoromethane;
DOI:10.1002/chem.201103221