trifluoro-methanesulfonic acid 4-(2-methoxycarbonyloxy-ethyl)-3-methyl-1-(toluene-4-sulfonyl)-1H-indol-5-yl ester

Base Information

Chemical Name:trifluoro-methanesulfonic acid 4-(2-methoxycarbonyloxy-ethyl)-3-methyl-1-(toluene-4-sulfonyl)-1H-indol-5-yl ester
CAS No.:869468-99-5
Molecular Formula:C₂₁H₂₀F₃NO₈S₂
Molecular Weight:535.519
Hs Code.:

trifluoro-methanesulfonic acid 4-(2-methoxycarbonyloxy-ethyl)-3-methyl-1-(toluene-4-sulfonyl)-1<i>H</i>-indol-5-yl ester

Synonyms:trifluoro-methanesulfonic acid 4-(2-methoxycarbonyloxy-ethyl)-3-methyl-1-(toluene-4-sulfonyl)-1H-indol-5-yl ester

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Chemical Property of trifluoro-methanesulfonic acid 4-(2-methoxycarbonyloxy-ethyl)-3-methyl-1-(toluene-4-sulfonyl)-1H-indol-5-yl ester

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Technology Process of trifluoro-methanesulfonic acid 4-(2-methoxycarbonyloxy-ethyl)-3-methyl-1-(toluene-4-sulfonyl)-1H-indol-5-yl ester

There total 2 articles about trifluoro-methanesulfonic acid 4-(2-methoxycarbonyloxy-ethyl)-3-methyl-1-(toluene-4-sulfonyl)-1H-indol-5-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: trifluoro-methanesulfonic acid 4-(2-hydroxy-ethyl)-3-methyl-1-(toluene-4-sulfonyl)-1H-indol-5-yl ester

: 79-22-1
methyl chloroformate

: 869468-99-5
trifluoro-methanesulfonic acid 4-(2-methoxycarbonyloxy-ethyl)-3-methyl-1-(toluene-4-sulfonyl)-1H-indol-5-yl ester

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 15h;
DOI:10.1021/ol052086c

Reference yield:

: 863582-36-9
trifluoro-methanesulfonic acid 3-methyl-4-(2-oxo-ethyl)-1-(toluene-4-sulfonyl)-1H-indol-5-yl ester

: 869468-99-5
trifluoro-methanesulfonic acid 4-(2-methoxycarbonyloxy-ethyl)-3-methyl-1-(toluene-4-sulfonyl)-1H-indol-5-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / methanol; tetrahydrofuran / 0.5 h / 0 °C

2: 1.53 g / pyridine / CH₂Cl₂ / 15 h / 20 °C

With pyridine; sodium tetrahydroborate; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ol052086c

Reference yield: 96.0%

: 869468-99-5
trifluoro-methanesulfonic acid 4-(2-methoxycarbonyloxy-ethyl)-3-methyl-1-(toluene-4-sulfonyl)-1H-indol-5-yl ester

: 55-21-0,27208-38-4
benzamide

: [8-methyl-6-(toluene-4-sulfonyl)-1,6-dihydro-2H-3,6-diaza-as-indacen-3-yl]-phenyl-methanone

Guidance literature:: With tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; at 110 ℃; for 20h;
DOI:10.1021/ol052086c