p-Tolyl O-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(1->4)-O-(2,3,6-tri-O-benzyl-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:p-Tolyl O-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(1->4)-O-(2,3,6-tri-O-benzyl-1-thio-β-D-glucopyranoside
CAS No.:172949-32-5
Molecular Formula:C₆₈H₇₀O₁₀S
Molecular Weight:1079.36
Hs Code.:

Synonyms:p-Tolyl O-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(1->4)-O-(2,3,6-tri-O-benzyl-1-thio-β-D-glucopyranoside

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Chemical Property of p-Tolyl O-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(1->4)-O-(2,3,6-tri-O-benzyl-1-thio-β-D-glucopyranoside

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Technology Process of p-Tolyl O-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(1->4)-O-(2,3,6-tri-O-benzyl-1-thio-β-D-glucopyranoside

There total 1 articles about p-Tolyl O-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(1->4)-O-(2,3,6-tri-O-benzyl-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 100-39-0
benzyl bromide

: 27894-74-2
4-methylphenyl (β-D-galactopyranosyl)-(1->4)-1-thio-β-D-glucopyranoside

: 172949-32-5
p-Tolyl O-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(1->4)-O-(2,3,6-tri-O-benzyl-1-thio-β-D-glucopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; for 6h; Ambient temperature;

Reference yield: 80.0%

: 617-86-7
triethylsilane

: 172949-32-5
p-Tolyl O-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(1->4)-O-(2,3,6-tri-O-benzyl-1-thio-β-D-glucopyranoside

: 1206803-46-4
p-methylphenyl (2,3,4,6-tetra-O-benzyl-β-D-galactospyranosyl)-(1->4)-2,3-di-O-benzyl-6-O-triethyl-silyl-1-thio-β-D-glucopyranoside

Guidance literature:: triethylsilane; With dicobalt octacarbonyl; carbon monoxide; at 20 ℃; for 0.25h; under 760.051 Torr;

p-Tolyl O-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(1->4)-O-(2,3,6-tri-O-benzyl-1-thio-β-D-glucopyranoside; In benzene; at 50 ℃; for 24h; regioselective reaction;
DOI:10.1021/ol902717y

Reference yield: 65.0%

: 172949-32-5
p-Tolyl O-(2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl)-(1->4)-O-(2,3,6-tri-O-benzyl-1-thio-β-D-glucopyranoside

: 1-deoxy-2,3,6-tri-O-benzyl-4-O-(2,3,4,6-tetra-O-benzyl-D-galactopyranosyl)-1-D-glucopyranose

Guidance literature:: With diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate; In 1,4-dioxane; for 1.5h; Inert atmosphere; UV-irradiation;
DOI:10.1080/07328303.2021.2015366