4,6-Bis(N,N-diethylcarbamoyl)-8-hydroxy-9,11-dimethyl-7-nitro-2-phenyl-5H-oxazolo<4,5-b>phenoxazine

Base Information

Chemical Name:4,6-Bis(N,N-diethylcarbamoyl)-8-hydroxy-9,11-dimethyl-7-nitro-2-phenyl-5H-oxazolo<4,5-b>phenoxazine
CAS No.:74273-69-1
Molecular Formula:C₃₁H₃₃N₅O₇
Molecular Weight:587.632
Hs Code.:

Synonyms:4,6-Bis(N,N-diethylcarbamoyl)-8-hydroxy-9,11-dimethyl-7-nitro-2-phenyl-5H-oxazolo<4,5-b>phenoxazine

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Chemical Property of 4,6-Bis(N,N-diethylcarbamoyl)-8-hydroxy-9,11-dimethyl-7-nitro-2-phenyl-5H-oxazolo<4,5-b>phenoxazine

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Technology Process of 4,6-Bis(N,N-diethylcarbamoyl)-8-hydroxy-9,11-dimethyl-7-nitro-2-phenyl-5H-oxazolo<4,5-b>phenoxazine

There total 2 articles about 4,6-Bis(N,N-diethylcarbamoyl)-8-hydroxy-9,11-dimethyl-7-nitro-2-phenyl-5H-oxazolo<4,5-b>phenoxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 74273-64-6
2-Amino-1,9-bis(N,N-diethylcarbamoyl)-7-hydroxy-4,6-dimethyl-8-nitro-3H-3-oxophenoxazine

: 100-52-7
benzaldehyde

: 74273-69-1
4,6-Bis(N,N-diethylcarbamoyl)-8-hydroxy-9,11-dimethyl-7-nitro-2-phenyl-5H-oxazolo<4,5-b>phenoxazine

Guidance literature:: at 180 ℃; for 5h;
DOI:10.1002/jhet.5570170104

Reference yield:

: 57270-61-8
2-amino-7-hydroxy-4,6-dimethyl-3-oxo-3H-phenoxazine-1,9-dicarboxylic acid bis-diethylamide

: 74273-69-1
4,6-Bis(N,N-diethylcarbamoyl)-8-hydroxy-9,11-dimethyl-7-nitro-2-phenyl-5H-oxazolo<4,5-b>phenoxazine

Guidance literature:: Multi-step reaction with 2 steps

1: 42 percent / 5percent aq. NaNO₂ / ethyl acetate; acetic acid / 0.5 h / 0 °C

2: 40 percent / 5 h / 180 °C

With sodium nitrite; In acetic acid; ethyl acetate;
DOI:10.1002/jhet.5570170104