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Technology Process of Tl(1+)*C6H5B(CH2P(C(CH3)3)2)2C3H(CH3)2N2(1-)=TlC6H5B(CH2P(C(CH3)3)2)2C3H(CH3)2N2

Tl(1+)*C6H5B(CH2P(C(CH3)3)2)2C3H(CH3)2N2(1-)=TlC6H5B(CH2P(C(CH3)3)2)2C3H(CH3)2N2

Base Information
  • Chemical Name:Tl(1+)*C6H5B(CH2P(C(CH3)3)2)2C3H(CH3)2N2(1-)=TlC6H5B(CH2P(C(CH3)3)2)2C3H(CH3)2N2
  • CAS No.:887368-20-9
  • Molecular Formula:C29H52BN2P2*Tl
  • Molecular Weight:705.887
  • Hs Code.:
Tl<sup>(1+)</sup>*C<sub>6</sub>H<sub>5</sub>B(CH<sub>2</sub>P(C(CH<sub>3</sub>)3)2)2C<sub>3</sub>H(CH<sub>3</sub>)2N<sub>2</sub><sup>(1-)</sup>=TlC<sub>6</sub>H<sub>5</sub>B(CH<sub>2</sub>P(C(CH<sub>3</sub>)3)2)2C<sub>3</sub>H(CH<sub>3</sub>)2N<sub>2</sub>

Synonyms:Tl(1+)*C6H5B(CH2P(C(CH3)3)2)2C3H(CH3)2N2(1-)=TlC6H5B(CH2P(C(CH3)3)2)2C3H(CH3)2N2

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Chemical Property of Tl(1+)*C6H5B(CH2P(C(CH3)3)2)2C3H(CH3)2N2(1-)=TlC6H5B(CH2P(C(CH3)3)2)2C3H(CH3)2N2
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Technology Process of Tl(1+)*C6H5B(CH2P(C(CH3)3)2)2C3H(CH3)2N2(1-)=TlC6H5B(CH2P(C(CH3)3)2)2C3H(CH3)2N2

There total 3 articles about Tl(1+)*C6H5B(CH2P(C(CH3)3)2)2C3H(CH3)2N2(1-)=TlC6H5B(CH2P(C(CH3)3)2)2C3H(CH3)2N2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenylborondichloride
873-51-8

phenylborondichloride

Tl<sup>(1+)</sup>*C<sub>6</sub>H<sub>5</sub>B(CH<sub>2</sub>P(C(CH<sub>3</sub>)3)2)2C<sub>3</sub>H(CH<sub>3</sub>)2N<sub>2</sub><sup>(1-)</sup>=TlC<sub>6</sub>H<sub>5</sub>B(CH<sub>2</sub>P(C(CH<sub>3</sub>)3)2)2C<sub>3</sub>H(CH<sub>3</sub>)2N<sub>2</sub>
887368-20-9

Tl(1+)*C6H5B(CH2P(C(CH3)3)2)2C3H(CH3)2N2(1-)=TlC6H5B(CH2P(C(CH3)3)2)2C3H(CH3)2N2

Guidance literature:
Multi-step reaction with 2 steps
1: diethyl ether
2: not given
In diethyl ether;
DOI:10.1021/ja0604358

Reference yield:

(lithiomethyl)bis(tert-butyl)phosphane
64065-07-2

(lithiomethyl)bis(tert-butyl)phosphane

Tl<sup>(1+)</sup>*C<sub>6</sub>H<sub>5</sub>B(CH<sub>2</sub>P(C(CH<sub>3</sub>)3)2)2C<sub>3</sub>H(CH<sub>3</sub>)2N<sub>2</sub><sup>(1-)</sup>=TlC<sub>6</sub>H<sub>5</sub>B(CH<sub>2</sub>P(C(CH<sub>3</sub>)3)2)2C<sub>3</sub>H(CH<sub>3</sub>)2N<sub>2</sub>
887368-20-9

Tl(1+)*C6H5B(CH2P(C(CH3)3)2)2C3H(CH3)2N2(1-)=TlC6H5B(CH2P(C(CH3)3)2)2C3H(CH3)2N2

Guidance literature:
Multi-step reaction with 2 steps
1: diethyl ether
2: not given
In diethyl ether;
DOI:10.1021/ja0604358

Reference yield:

PhB(CH<sub>2</sub>P((t)Bu)2)2
820219-05-4

PhB(CH2P((t)Bu)2)2

thallium(I) hexafluorophosphate
60969-19-9

thallium(I) hexafluorophosphate

3,5-dimethylpyrazolate lithium salt

3,5-dimethylpyrazolate lithium salt

Tl<sup>(1+)</sup>*C<sub>6</sub>H<sub>5</sub>B(CH<sub>2</sub>P(C(CH<sub>3</sub>)3)2)2C<sub>3</sub>H(CH<sub>3</sub>)2N<sub>2</sub><sup>(1-)</sup>=TlC<sub>6</sub>H<sub>5</sub>B(CH<sub>2</sub>P(C(CH<sub>3</sub>)3)2)2C<sub>3</sub>H(CH<sub>3</sub>)2N<sub>2</sub>
887368-20-9

Tl(1+)*C6H5B(CH2P(C(CH3)3)2)2C3H(CH3)2N2(1-)=TlC6H5B(CH2P(C(CH3)3)2)2C3H(CH3)2N2

Guidance literature:
In not given;
DOI:10.1021/ja0604358
upstream raw materials:

PhB(CH2P((t)Bu)2)2

thallium(I) hexafluorophosphate

(lithiomethyl)bis(tert-butyl)phosphane

phenylborondichloride

Downstream raw materials:

FeCl(C6H5B(CH2P(C(CH3)3)2)2C3H(CH3)2N2)

FeP(CH3)3(C6H5B(CH2P(C(CH3)3)2)2C3H(CH3)2N2)

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