N,N'-dibenzyl-benzene-1,3-dicarbothioamide

Base Information

Chemical Name:N,N'-dibenzyl-benzene-1,3-dicarbothioamide
CAS No.:1047661-71-1
Molecular Formula:C₂₂H₂₀N₂S₂
Molecular Weight:376.546
Hs Code.:

Synonyms:N,N'-dibenzyl-benzene-1,3-dicarbothioamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-dibenzyl-benzene-1,3-dicarbothioamide

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Technology Process of N,N'-dibenzyl-benzene-1,3-dicarbothioamide

There total 1 articles about N,N'-dibenzyl-benzene-1,3-dicarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 626-19-7
Isophthalaldehyde

: 100-46-9
benzylamine

: 1047661-71-1
N,N'-dibenzyl-benzene-1,3-dicarbothioamide

Guidance literature:: With sulfur; In N,N-dimethyl-formamide; at 75 ℃; for 3h;
DOI:10.1246/cl.2008.646

Reference yield: 89.0%

: 10025-99-7
potassium tetrachloroplatinate(II)

: 1047661-71-1
N,N'-dibenzyl-benzene-1,3-dicarbothioamide

: 1155859-67-8
[2,6-bis(benzylaminothiocarbonyl)-κ2S,S'-phenyl-κC1]chloroplatinum(II)

Guidance literature:: In acetic acid; refluxing mixt. of platinum compd., thioamide deriv. and acetic acid for72 h; filtration, washing with methanol and water, elem. anal.;
DOI:10.1021/om800894j

Reference yield: 77.0%

: 13462-90-3
nickel(II) iodide

: 1047661-71-1
N,N'-dibenzyl-benzene-1,3-dicarbothioamide

: 1246009-70-0
[2,6-bis(benzylaminothiocarbonyl)-κ2-S,S'-phenyl-κ1-C1]iodonickel(II)

Guidance literature:: In toluene; mixt. of Ni salt and benzene deriv. (1:1) in toluene stirred at 110°C for 72 h; ppt. filtered off, washed hexane and EtOH, dried under vac.; elem. anal.;
DOI:10.1016/j.ica.2010.04.012