tetrakis-(5-methyl-2-(4-phenylphenyl)pyridine(-1H))-μ-(dichloro)-diiridium(III)

Base Information

Chemical Name:tetrakis-(5-methyl-2-(4-phenylphenyl)pyridine(-1H))-μ-(dichloro)-diiridium(III)
CAS No.:808142-75-8
Molecular Formula:C₇₂H₅₆Cl₂Ir₂N₄
Molecular Weight:1432.61
Hs Code.:

Synonyms:tetrakis-(5-methyl-2-(4-phenylphenyl)pyridine(-1H))-μ-(dichloro)-diiridium(III)

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Chemical Property of tetrakis-(5-methyl-2-(4-phenylphenyl)pyridine(-1H))-μ-(dichloro)-diiridium(III)

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Technology Process of tetrakis-(5-methyl-2-(4-phenylphenyl)pyridine(-1H))-μ-(dichloro)-diiridium(III)

There total 3 articles about tetrakis-(5-methyl-2-(4-phenylphenyl)pyridine(-1H))-μ-(dichloro)-diiridium(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.9%

: iridium(III) chloride trihydrate

: 808142-70-3
5-methyl-2-(4-phenylphenyl)pyridine

: 808142-75-8
tetrakis-(5-methyl-2-(4-phenylphenyl)pyridine(-1H))-μ-(dichloro)-diiridium(III)

Guidance literature:: In 2-ethoxy-ethanol; water; for 24h; Inert atmosphere;

Reference yield:

: iridium(III) chloride trihydrate hydrochloride

: 808142-70-3
5-methyl-2-(4-phenylphenyl)pyridine

: 808142-75-8
tetrakis-(5-methyl-2-(4-phenylphenyl)pyridine(-1H))-μ-(dichloro)-diiridium(III)

Guidance literature:: In 2-methoxy-ethanol; water; ligand added to Ir salt in methoxyethanol/H2O, refluxed for 12 h; filtered, washed (H2O and Et2O), dried;
DOI:10.1021/ja047156+

Reference yield:

: iridium(III) chloride hydrate

: 808142-70-3
5-methyl-2-(4-phenylphenyl)pyridine

: 808142-75-8
tetrakis-(5-methyl-2-(4-phenylphenyl)pyridine(-1H))-μ-(dichloro)-diiridium(III)

Guidance literature:: In 2-methoxy-ethanol; water; mixt. of 2.1 equiv. of pyridine deriv. and iridium compd. (ratio = 3:1) in 2-methoxyethanol/water heated at 125°C for 18 h; cooling, addn. of water, solid vac.-filtered, washed with water and hexane, dried under vac.;
DOI:10.1021/ic701747j