(6R)-6-{(2S)-4-[4-(benzyloxy)phenyl]-2-{[(tert-butyl)dimethylsilyl]oxy}butyl}-5,6-dihydro-2H-pyran-2-one

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Chemical Name:(6R)-6-{(2S)-4-[4-(benzyloxy)phenyl]-2-{[(tert-butyl)dimethylsilyl]oxy}butyl}-5,6-dihydro-2H-pyran-2-one
CAS No.:1187819-87-9
Molecular Formula:C₂₈H₃₈O₄Si
Molecular Weight:466.693
Hs Code.:

Synonyms:(6R)-6-{(2S)-4-[4-(benzyloxy)phenyl]-2-{[(tert-butyl)dimethylsilyl]oxy}butyl}-5,6-dihydro-2H-pyran-2-one

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Chemical Property of (6R)-6-{(2S)-4-[4-(benzyloxy)phenyl]-2-{[(tert-butyl)dimethylsilyl]oxy}butyl}-5,6-dihydro-2H-pyran-2-one

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Technology Process of (6R)-6-{(2S)-4-[4-(benzyloxy)phenyl]-2-{[(tert-butyl)dimethylsilyl]oxy}butyl}-5,6-dihydro-2H-pyran-2-one

There total 1 articles about (6R)-6-{(2S)-4-[4-(benzyloxy)phenyl]-2-{[(tert-butyl)dimethylsilyl]oxy}butyl}-5,6-dihydro-2H-pyran-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1187819-77-7
(1R,3S)-5-[4-(benzyloxy)phenyl]-3-{[(tert-butyl)dimethylsilyl]oxy}-1-(prop-2-en-1-yl)pentyl prop-2-enoate

: 1187819-87-9
(6R)-6-{(2S)-4-[4-(benzyloxy)phenyl]-2-{[(tert-butyl)dimethylsilyl]oxy}butyl}-5,6-dihydro-2H-pyran-2-one

Guidance literature:: With Grubbs catalyst first generation; In dichloromethane; at 55 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.tetasy.2009.05.036

Reference yield: 89.0%

: 1187819-87-9
(6R)-6-{(2S)-4-[4-(benzyloxy)phenyl]-2-{[(tert-butyl)dimethylsilyl]oxy}butyl}-5,6-dihydro-2H-pyran-2-one

: 1004519-87-2
(R)-6-((S)-2-hydroxy-4-(4-hydroxyphenyl)butyl)-5,6-dihydropyran-2-one

Guidance literature:: (6R)-6-{(2S)-4-[4-(benzyloxy)phenyl]-2-{[(tert-butyl)dimethylsilyl]oxy}butyl}-5,6-dihydro-2H-pyran-2-one; With titanium tetrachloride; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

With water; sodium hydrogencarbonate; In dichloromethane; Inert atmosphere;
DOI:10.1016/j.tetasy.2009.05.036