(1R,3S)-5-[4-(benzyloxy)phenyl]-3-{[(tert-butyl)dimethylsilyl]oxy}-1-(prop-2-en-1-yl)pentyl prop-2-enoate

Base Information

Chemical Name:(1R,3S)-5-[4-(benzyloxy)phenyl]-3-{[(tert-butyl)dimethylsilyl]oxy}-1-(prop-2-en-1-yl)pentyl prop-2-enoate
CAS No.:1187819-77-7
Molecular Formula:C₃₀H₄₂O₄Si
Molecular Weight:494.747
Hs Code.:

Synonyms:(1R,3S)-5-[4-(benzyloxy)phenyl]-3-{[(tert-butyl)dimethylsilyl]oxy}-1-(prop-2-en-1-yl)pentyl prop-2-enoate

Suppliers and Price of (1R,3S)-5-[4-(benzyloxy)phenyl]-3-{[(tert-butyl)dimethylsilyl]oxy}-1-(prop-2-en-1-yl)pentyl prop-2-enoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,3S)-5-[4-(benzyloxy)phenyl]-3-{[(tert-butyl)dimethylsilyl]oxy}-1-(prop-2-en-1-yl)pentyl prop-2-enoate

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Technology Process of (1R,3S)-5-[4-(benzyloxy)phenyl]-3-{[(tert-butyl)dimethylsilyl]oxy}-1-(prop-2-en-1-yl)pentyl prop-2-enoate

There total 1 articles about (1R,3S)-5-[4-(benzyloxy)phenyl]-3-{[(tert-butyl)dimethylsilyl]oxy}-1-(prop-2-en-1-yl)pentyl prop-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1187819-78-8
(4R,6S)-8-[4-(benzyloxy)phenyl]-6-{[(tert-butyl)dimethylsilyl]oxy}oct-1-en-4-ol

: 814-68-6,25189-84-8
acryloyl chloride

: 1187819-77-7
(1R,3S)-5-[4-(benzyloxy)phenyl]-3-{[(tert-butyl)dimethylsilyl]oxy}-1-(prop-2-en-1-yl)pentyl prop-2-enoate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tetasy.2009.05.036

Reference yield: 85.0%

: 1187819-77-7
(1R,3S)-5-[4-(benzyloxy)phenyl]-3-{[(tert-butyl)dimethylsilyl]oxy}-1-(prop-2-en-1-yl)pentyl prop-2-enoate

: 1187819-87-9
(6R)-6-{(2S)-4-[4-(benzyloxy)phenyl]-2-{[(tert-butyl)dimethylsilyl]oxy}butyl}-5,6-dihydro-2H-pyran-2-one

Guidance literature:: With Grubbs catalyst first generation; In dichloromethane; at 55 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.tetasy.2009.05.036