tert-butyl((4,5-dimethylfuran-2-yl)(2-ethynylphenyl)methoxy)dimethylsilane

Base Information

Chemical Name:tert-butyl((4,5-dimethylfuran-2-yl)(2-ethynylphenyl)methoxy)dimethylsilane
CAS No.:1443751-11-8
Molecular Formula:C₂₁H₂₈O₂Si
Molecular Weight:340.538
Hs Code.:

Synonyms:tert-butyl((4,5-dimethylfuran-2-yl)(2-ethynylphenyl)methoxy)dimethylsilane

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Chemical Property of tert-butyl((4,5-dimethylfuran-2-yl)(2-ethynylphenyl)methoxy)dimethylsilane

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Technology Process of tert-butyl((4,5-dimethylfuran-2-yl)(2-ethynylphenyl)methoxy)dimethylsilane

There total 2 articles about tert-butyl((4,5-dimethylfuran-2-yl)(2-ethynylphenyl)methoxy)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1443751-07-2
(4,5-dimethylfuran-2-yl)(2-ethynylphenyl)methanol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1443751-11-8
tert-butyl((4,5-dimethylfuran-2-yl)(2-ethynylphenyl)methoxy)dimethylsilane

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 24h;
DOI:10.1002/chem.201202004

Reference yield:

: 38274-16-7
2-bromo-1-(trimethylsilylethynyl)benzene

: 1443751-11-8
tert-butyl((4,5-dimethylfuran-2-yl)(2-ethynylphenyl)methoxy)dimethylsilane

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

1.2: 16 h / -78 - 20 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.08 h / 0 °C

3.1: 1H-imidazole / N,N-dimethyl-formamide / 24 h / 20 °C

With 1H-imidazole; n-butyllithium; tetrabutyl ammonium fluoride; In tetrahydrofuran; hexane; N,N-dimethyl-formamide;
DOI:10.1002/chem.201202004