3'-nitroapigenin

Base Information

• Chemical Name: 3'-nitroapigenin
• CAS No.: 890661-83-3
• Molecular Formula: C₁₅H₉NO₇
• Molecular Weight: 315.239
• Mol file: 890661-83-3.mol

Synonyms:3'-nitroapigenin

Chemical Property of 3'-nitroapigenin

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 3'-nitroapigenin

There total 3 articles about 3'-nitroapigenin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5,7-dihydroxy-2-(4-hydroxyphenyl)-4H-1-benzopyran-4-one (520-36-5) → 3'-nitroapigenin (890661-83-3)

Guidance literature:

With potassium hydroxide; tetranitromethane; In water; dimethyl sulfoxide; at 5 - 20 ℃;

Reference yield:

3'-nitrorhoifolin (890661-82-2) → 3'-nitroapigenin (890661-83-3)

Guidance literature:

With hydrogenchloride; In water; at 20 - 55 ℃; for 4h;

DOI:10.1016/j.tet.2006.02.024

Reference yield:

rhoifolin (17306-46-6) → 3'-nitroapigenin (890661-83-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / HNO₃; TFA / 2 h / 0 °C

2: 131 mg / HCl / H₂O / 4 h / 20 - 55 °C

With hydrogenchloride; nitric acid; trifluoroacetic acid; In water;

DOI:10.1016/j.tet.2006.02.024

upstream raw materials:

3'-nitrorhoifolin

rhoifolin

5,7-dihydroxy-2-(4-hydroxyphenyl)-4H-1-benzopyran-4-one

Downstream raw materials:

C₁₅H₁₁NO₅