C₁₀H₁₁ClF₂O

Base Information

Chemical Name:C₁₀H₁₁ClF₂O
CAS No.:798564-58-6
Molecular Formula:C₁₀H₁₁ClF₂O
Molecular Weight:220.647
Hs Code.:

C<sub>10</sub>H<sub>11</sub>ClF<sub>2</sub>O

Synonyms:C₁₀H₁₁ClF₂O

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Chemical Property of C₁₀H₁₁ClF₂O

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Technology Process of C₁₀H₁₁ClF₂O

There total 3 articles about C₁₀H₁₁ClF₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 798564-57-5
C₁₀H₁₂F₂O₂

: 798564-58-6
C₁₀H₁₁ClF₂O

Guidance literature:: With methanesulfonyl chloride; triethylamine; In dichloromethane; at 20 - 40 ℃; for 23.1667h; Heating / reflux;

Reference yield:

: 203059-83-0
1,3-difluoro-4-isopropoxybenzene

: 798564-58-6
C₁₀H₁₁ClF₂O

Guidance literature:: Multi-step reaction with 3 steps

1.1: sec.-butyllithium / tetrahydrofuran; cyclohexane / 0.5 h / -78 - -75 °C

1.2: 0.67 h / -40 - 0 °C

2.1: lithium aluminium tetrahydride; ammonium chloride / tetrahydrofuran / 0.5 h / 0 - 45 °C

3.1: methanesulfonyl chloride; triethylamine / dichloromethane / 23.17 h / 20 - 40 °C / Heating / reflux

With lithium aluminium tetrahydride; sec.-butyllithium; ammonium chloride; methanesulfonyl chloride; triethylamine; In tetrahydrofuran; dichloromethane; cyclohexane;

Reference yield:

: 367-27-1
2,4-difluorophenol

: 798564-58-6
C₁₀H₁₁ClF₂O

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / acetone / 20 h / Heating / reflux

2.1: sec.-butyllithium / tetrahydrofuran; cyclohexane / 0.5 h / -78 - -75 °C

2.2: 0.67 h / -40 - 0 °C

3.1: lithium aluminium tetrahydride; ammonium chloride / tetrahydrofuran / 0.5 h / 0 - 45 °C

4.1: methanesulfonyl chloride; triethylamine / dichloromethane / 23.17 h / 20 - 40 °C / Heating / reflux

With lithium aluminium tetrahydride; sec.-butyllithium; potassium carbonate; ammonium chloride; methanesulfonyl chloride; triethylamine; In tetrahydrofuran; dichloromethane; cyclohexane; acetone;