chlorobis(dimethylglyoximato)(triphenylphosphine)cobalt

Base Information

• Chemical Name: chlorobis(dimethylglyoximato)(triphenylphosphine)cobalt
• CAS No.: 23295-34-3
• Molecular Formula: C₂₆H₂₉ClCoN₄O₄P
• Molecular Weight: 586.961

Synonyms:chlorobis(dimethylglyoximato)(triphenylphosphine)cobalt

Chemical Property of chlorobis(dimethylglyoximato)(triphenylphosphine)cobalt

Chemical Property:

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Technology Process of chlorobis(dimethylglyoximato)(triphenylphosphine)cobalt

There total 3 articles about chlorobis(dimethylglyoximato)(triphenylphosphine)cobalt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

PPh3Co(DH)2N3 (69879-86-3) → chlorobis(dimethylglyoximato)(triphenylphosphine)cobalt (23295-34-3)

Guidance literature:

With hydrogenchloride; In acetone; HCl gas bubbled through acetone PPh3Co(DH)2N3; elem. anal.;

DOI:10.1021/ic00133a069

Reference yield: 18.0%

(C6H5)3PCo(HONC(CH3)C(CH3)NO)2(N3C2)(CO2CH3)2 (80462-11-9) → chlorobis(dimethylglyoximato)(triphenylphosphine)cobalt (23295-34-3) + dimethyl 2H-1,2,3-triazole-4,5-dicarboxylate (707-94-8)

Guidance literature:

With hydrogenchloride; In acetone; to soln. (CH3CO2)2(C2N3)Co(DH)2PPh3 in acetone added concd. HCl and soln. stirred for 2 days at room temp.; crystals filtered, washed with abs. ethanol and petroleum ether and air-dried;

DOI:10.1021/ic00133a069

Reference yield:

[Co(CH3C(NOH)C(NO)CH3)2(P(C6H5)3)] (36451-59-9) → [CoCl(CH3C(NOH)C(NO)CH3)2(P(C6H5)3)] (23295-34-3)

Guidance literature:

With tetrachloromethane; In benzene; byproducts: CCl3 radical; 19.67-34.44°C; Kinetics;

upstream raw materials:

PPh₃Co(DH)2N₃

(C₆H₅)3PCo(HONC(CH₃)C(CH₃)NO)2(N₃C₂)(CO₂CH₃)2

[Co(CH₃C(NOH)C(NO)CH₃)2(P(C₆H₅)3)]

Downstream raw materials:

Co(ONC(CH₃)C(CH₃)NOH)2(P(C₆H₅)3)I

bis(dimethylglyoximato)(triphenylphosphine)(3-fluoropropyl)cobalt

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